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Preparation of alpha-5-aza-2'-deoxy-[6-3H]cytidine

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    0312028 - ÚOCHB 2009 RIV CZ eng J - Journal Article
    Elbert, Tomáš - Černý, B.
    Preparation of alpha-5-aza-2'-deoxy-[6-3H]cytidine.
    [Příprava alfa-5aza-2'-deoxy-[6-3H]cytidinu.]
    Collection of Czechoslovak Chemical Communications. Roč. 73, č. 5 (2008), s. 701-704. ISSN 0010-0765
    Institutional research plan: CEZ:AV0Z40550506
    Keywords : alfa-5aza-2'-deoxy-cytidine
    Subject RIV: CC - Organic Chemistry
    Impact factor: 0.784, year: 2008

    alpha-5-Aza-2'-deoxy-cytidine was labeled by tritium on the C-6 of the heterocyclic triazine ring. The structure of the labeled compound was proved by 3H and 1H NMR. The specific activity was 0.71 TBq/mmol (19.2 Ci/mmol) and radiochemical purity was > 99%. The long term stability of the product during storage at -21 and -72 °C was followed by radio-HPLC.

    alfa-5-Aza-2'-deoxy-cytidin byl označen tritiem na C-6 triazinového heterocyklického kruhu. Struktura značené látky byla prokázána 3H a 1H NMR spektry. Specifická aktivita byla 0,71 TBq/mmol (19,2 Ci/mmol) a radiochemická čistota byla > 99%. Stabilita značené látky během skladování při -21 a -72 °C byla sledována radio-HPLC.
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