(H.sub.3./sub.dien)[Ni(NO.sub.3./sub.)(C.sub.2./sub.O.sub.4./sub.).sub.2./sub.].2H.sub.2./sub.O: Synthesis, crystal structure, catalytic activity and magnetic study

0564749 - FZÚ 2023 RIV NL eng J - Journal Article
Akouibaa, M. - Hassani, H.O. - Ouarsal, R. - Rakib, S. - Lachkar, M. - Poupon, Morgane - Dušek, Michal - Morley, N. - El Bali, B.
(H₃dien)[Ni(NO₃)(C₂O₄)₂].2H₂O: Synthesis, crystal structure, catalytic activity and magnetic study.
Chemical Data Collections. Roč. 42, Dec. (2022), č. článku 100969. ISSN 2405-8300
R&D Projects: GA ČR(CZ) GA18-10504S
Research Infrastructure: CzechNanoLab - 90110
Institutional support: RVO:68378271
Keywords : hybrid material * crystal structure * spectroscopy * magnetism * catalysis
OECD category: Condensed matter physics (including formerly solid state physics, supercond.)
Method of publishing: Limited access
https://doi.org/10.1016/j.cdc.2022.100969

The complex (H3dien)[Ni(NO3)(C2O4)2].2H2O, with (dien) is the diethylenetriamine (NH2CH2CH2)2NH, and was synthesized in solution. It was characterized using single-crystal X-ray diffraction, Infrared (FT-IR) and UV-Visible spectroscopies, and TG-DTA thermal analysis. FT-IR confirmed the characteristic bands of diethylenetriamine, nitrate and oxalate groups.
Permanent Link: https://hdl.handle.net/11104/0336418