Effect of Short Attritor-Milling of Magnesium Alloy Powder Prior to Spark Plasma Sintering

0534277 - ÚJF 2021 RIV CH eng J - Journal Article
Minárik, P. - Zemková, M. - Knapek, Michal - Šašek, S. - Dittrich, J. - Lukáč, František - Kozlík, J. - Král, R.
Effect of Short Attritor-Milling of Magnesium Alloy Powder Prior to Spark Plasma Sintering.
Materials. Roč. 13, č. 18 (2020), č. článku 3973. E-ISSN 1996-1944
R&D Projects: GA MŠMT EF16_013/0001794
Institutional support: RVO:61389005 ; RVO:61389021
Keywords : Magnesium * powder * spark plasma sintering * milling * mechnical properties * microstructure
OECD category: Nuclear physics; Materials engineering (UFP-V)
Impact factor: 3.623, year: 2020
Method of publishing: Open access
https://doi.org/10.3390/ma13183973

The spark plasma sintering (SPS) technique was employed to prepare compacts from (i) gas-atomized and (ii) attritor-milled AE42 magnesium powder. Short attritor-milling was used mainly to disrupt the MgO shell covering the powder particles and, in turn, to enhance consolidation during sintering. Compacts prepared by SPS from the milled powder featured finer microstructures than compacts consolidated from gas-atomized powder (i.e., without milling), regardless of the sintering temperatures in the range of 400-550 degrees C. Furthermore, the grain growth associated with the increase in the sintering temperature in these samples was less pronounced than in the samples prepared from gas-atomized particles. Consequently, the mechanical properties were significantly enhanced in the material made of milled powder. Apart from grain refinement, the improvements in mechanical performance were attributed to the synergic effect of the irregular shape of the milled particles and better consolidation due to effectively disrupted MgO shells, thus suppressing the crack formation and propagation during loading. These results suggest that relatively short milling of magnesium alloy powder can be effectively used to achieve superior mechanical properties during consolidation by SPS even at relatively low temperatures.
Permanent Link: http://hdl.handle.net/11104/0312498