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Determination of Composition and Anomeric Ratio in Mixtures of Fluorinated Ologosaccharides.
- 1.0521796 - ÚCHP 2020 CZ eng C - Conference Paper (international conference)
Červenková Šťastná, Lucie - Kurfiřt, Martin - Hamala, Vojtěch - Karban, Jindřich
Determination of Composition and Anomeric Ratio in Mixtures of Fluorinated Ologosaccharides.
Book of Abstracts. Prague: Institute of Chemical Process Fundamentals of the CAS, v. v. i., 2019, s. 63, č. článku P17. ISBN 978-80-86186-97-9.
[Magnetic Moments in Central Europe 2019. Prague (CZ), 27.02.2019-03.03.2019]
R&D Projects: GA MŠMT(CZ) LM2015037
Institutional support: RVO:67985858
Keywords : deoxofluorinated oligosaccharides * glycosylation * 2D NMR techniques
OECD category: Organic chemistry
Plenthora of glycosylation reactions was performed and sophisticated NMR approach for characteriza-tion of the coressponding products was aplied. ID 19F and *H NMR were utilized for accurate derermina-tion of anomeric ratios and 2D NMR techniques as HSQC, HMBC and COSY were used to assign the signals of individual anomers. In some cases, spectrum simulation was necessary to obtain the desired parameters.
Permanent Link: http://hdl.handle.net/11104/0306362
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Number of the records: 1