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Characterization and crystal structures of new Schiff base macrocyclic compounds
- 1.0456817 - FZÚ 2016 RIV RU eng J - Journal Article
Khalaji, A.D. - Ghoran, S.H. - Pojarová, Michaela - Dušek, Michal
Characterization and crystal structures of new Schiff base macrocyclic compounds.
Journal of Structural Chemistry. Roč. 56, č. 7 (2015), s. 1410-1414. ISSN 0022-4766. E-ISSN 1573-8779
R&D Projects: GA ČR(CZ) GA14-03276S
Institutional support: RVO:68378271
Keywords : synthesis * macrocyclic Schiff base * single crystal structure analysis * spectroscopy
Subject RIV: BM - Solid Matter Physics ; Magnetism
Impact factor: 0.536, year: 2015
We report the synthesis and characterization of two new macrocyclic Schiff base compounds: a 15-membered (1) and 16-membered (2) one. Their synthesis involves a Schiff base condensation of 2,2-dimethylpropanediamine and two dialdehydes: 5,5′-dimethoxy-2,2′-(ethane-1,2-diyldioxy)dibenzaldehyde and 5,5′-dimethoxy-2,2′-(propane-1,3-diyldioxy)dibenzaldehyde. The compounds are characterized by elemental analysis (CHN), FT-IR, 1H and 13C-NMR spectroscopy, and single crystal X-ray diffraction.
Permanent Link: http://hdl.handle.net/11104/0257289
Number of the records: 1