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Tunable rapid microwave synthesis of up-converting hexagonal NaYxGdyYbzEr(1−x−y−z)F4 nanocrystals in large quantity

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    0455135 - FGÚ 2016 RIV CH eng J - Journal Article
    Bartůněk, V. - Pinc, J. - Ulbrich, P. - Rak, J. - Pelánková, B. - Král, V. - Kuchař, M. - Ježek, Petr - Engstová, Hana - Smolková, Katarína
    Tunable rapid microwave synthesis of up-converting hexagonal NaYxGdyYbzEr(1−x−y−z)F4 nanocrystals in large quantity.
    Journal of Fluorine Chemistry. Roč. 178, Oct 2015 (2015), s. 56-60. ISSN 0022-1139. E-ISSN 1873-3328
    R&D Projects: GA ČR(CZ) GA15-01897S; GA MŠMT(CZ) LF14001
    Institutional support: RVO:67985823
    Keywords : microwave syntheses * ionic liquid * rare earths * up-conversion * large amount
    Subject RIV: BO - Biophysics
    Impact factor: 2.213, year: 2015

    Various sizes of pure hexagonal nanocrystals of NaYxGdyYbzEr(1−x−y−z)F4 were prepared by simple synthesis using microwave radiation. Ionic liquid bmimCl was used as a solvent and NH4F as a fluorination agent. Nanocrystal sizes were controlled by varying water volume or by addition of various surfactants. The method is suitable even for preparation of large amounts of nanocrystals and could be easily modified and used for numerous related applications
    Permanent Link: http://hdl.handle.net/11104/0255783

     
     
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