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The labeling of brassinosteroids by tritium

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    0446829 - ÚOCHB 2016 RIV GB eng J - Journal Article
    Marek, Aleš - Patil, Mahadeo Rajshekhar - Elbert, Tomáš
    The labeling of brassinosteroids by tritium.
    RSC Advances. Roč. 5, č. 80 (2015), s. 65214-65220. E-ISSN 2046-2069
    R&D Projects: GA AV ČR IAA400550801
    Institutional support: RVO:61388963
    Keywords : brassinolide * hydrogen * isotopes
    Subject RIV: CC - Organic Chemistry
    Impact factor: 3.289, year: 2015

    A convenient method for the synthesis of tritium-labeled brassinosteroids with very high specific activity is reported. A H-3-labeled 24-epicastasterone was isolated in high yield (40 mCi), radiochemical purity (>97%) and a specific activity up to 99 Ci mmol(-1). The labeling strategy was designed to employ a radiolabeling step at the late stage of the synthetic sequence.
    Permanent Link: http://hdl.handle.net/11104/0248796

     
     
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