Structure of the high-temperature phase of caesium nitrate – the importance of high-resolution data

Fábry, J.; Kučeráková, M.; Dušek, M.; Buixaderas, E.; Hlinka, J.

doi:10.1107/S2052520622001135

Structure of the high-temperature phase of caesium nitrate – the importance of high-resolution data

J. Fábry, M. Kučeráková, M. Dušek, E. Buixaderas and J. Hlinka

A single-crystal structure determination of the cubic phase of CsNO₃ based on data collected at 439 K up to sinθ_max/λ = 0.995000 Å⁻¹, i.e. to an unprecedentedly high-θ value, is reported. The structure has been refined in Pm3m (Z = 1). Analysis of the difference electron-density maps revealed that the most appropriate model is the twelve-orientation model with the Cs, N, O1 and O2 atoms situated on the Wyckoff positions 1a, 6f, 6f and 24l, respectively, rather than the eight-orientation aragonite model with the Cs, N and O atoms situated on the Wyckoff positions 1a, 8g and 24m, respectively. Both models, however, show close similarities if the large anisotropic displacement parameters of the O atoms in the eight-orientation aragonite model are taken into account. The reason for this is shown to lie in the smeared electron density around the positions of the disordered [NO₃]⁻ anion.

Keywords: alkali nitrates; positional disorder; twelve-orientation model; eight-orientation aragonite model; difference electron-density maps.

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Supporting information

	Crystallographic Information File (CIF) https://doi.org/10.1107/S2052520622001135/yv5002sup1.cif Contains datablocks global, I
	Structure factor file (CIF format) https://doi.org/10.1107/S2052520622001135/yv5002Isup2.hkl Contains datablock I
	Portable Document Format (PDF) file https://doi.org/10.1107/S2052520622001135/yv5002sup3.pdf Additional table and figures

CCDC reference: 2149583

Computing details top

Data collection: CrysAlis PRO (Rigaku OD, 2018); cell refinement: CrysAlis PRO (Rigaku OD, 2018); data reduction: CrysAlis PRO (Rigaku OD, 2018); program(s) used to solve structure: SUPERFLIP (Palatinus & Chapuis, 2007); program(s) used to refine structure: JANA2006 (Petříček et al., 2014); molecular graphics: Diamond 3.2e (Brandenburg, 2015); Mercury 4.0 (Macrae et al., 2020); software used to prepare material for publication: JANA2006.

caesium nitrate top

Crystal data top

CsNO₃	D_x = 3.499 Mg m⁻³
M_r = 194.9	Mo Kα radiation, λ = 0.71073 Å
Cubic, Pm3m	Cell parameters from 1623 reflections
Hall symbol: -P 4 2 3	θ = 4.5–44.1°
a = 4.5226 (6) Å	µ = 9.83 mm⁻¹
V = 92.50 (2) Å³	T = 440 K
Z = 1	Prism, colourless
F(000) = 86	0.39 × 0.09 × 0.08 mm

Data collection top

Xcalibur, AtlasS2, Gemini ultra diffractometer	109 independent reflections
Radiation source: X-ray tube	74 reflections with I > 3σ(I)
Graphite monochromator	R_int = 0.037
Detector resolution: 5.1783 pixels mm^-1	θ_max = 45.0°, θ_min = 4.5°
Oxford Diffraction CCD scans	h = −9→8
Absorption correction: multi-scan CrysAlisPro 1.171.41.93a (Rigaku Oxford Diffraction, 2020)	k = −8→9
T_min = 0.347, T_max = 0.464	l = −8→8
4035 measured reflections

Refinement top

Refinement on F²	2 restraints
R[F > 3σ(F)] = 0.014	0 constraints
wR(F) = 0.059	Weighting scheme based on measured s.u.'s w = 1/(σ²(I) + 0.0004I²)
S = 1.87	(Δ/σ)_max = 0.048
109 reflections	Δρ_max = 0.64 e Å⁻³
14 parameters	Δρ_min = −0.38 e Å⁻³

Special details top

Experimental. The crystals were first glued by Loctite EA 9492, Henkel, and then the joint was covered by Ceramobond 571, T-E Klebetechnik, Hannover.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq	Occ. (<1)
Cs1	0	0	0	0.06281 (15)
N1	0.5	0.5	0.551 (12)	0.10 (2)	0.1667
O1	0.5	0.5	0.837 (10)	0.060 (7)	0.1667
O2	0.751 (6)	0.5	0.414 (10)	0.098 (17)	0.0833

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Cs1	0.0628 (3)	0.0628 (3)	0.0628 (3)	0	0	0
N1	0.13 (4)	0.13 (4)	0.05 (3)	0	0	0
O1	0.053 (9)	0.053 (9)	0.072 (16)	0	0	0
O2	0.13 (4)	0.077 (17)	0.09 (3)	0	0.001 (18)	0

Geometric parameters (Å, º) top

N1—O1	1.29 (7)	Cs1—O2^xxxvi	3.15 (3)
N1—O2	1.29 (4)	Cs1—O2^xxxvii	3.15 (3)
N1—O2ⁱ	1.29 (4)	Cs1—O2^xxxviii	3.15 (3)
Cs1—O1ⁱⁱ	3.282 (11)	Cs1—O2^xxxix	3.15 (3)
Cs1—O1ⁱⁱⁱ	3.282 (11)	Cs1—O2^xl	3.15 (3)
Cs1—O1^iv	3.282 (11)	Cs1—O2^xli	3.15 (3)
Cs1—O1^v	3.282 (11)	Cs1—O2^xlii	3.15 (3)
Cs1—O1^vi	3.282 (11)	Cs1—O2^xliii	3.15 (3)
Cs1—O1^vii	3.282 (11)	Cs1—O2^xliv	3.15 (3)
Cs1—O1^viii	3.282 (11)	Cs1—O2^xlv	3.15 (3)
Cs1—O1^ix	3.282 (11)	Cs1—O2^xlvi	3.15 (3)
Cs1—O1^x	3.282 (11)	Cs1—O2^xlvii	3.15 (3)
Cs1—O1^xi	3.282 (11)	Cs1—O2^xlviii	3.15 (3)
Cs1—O1^xii	3.282 (11)	Cs1—O2^xlix	3.15 (3)
Cs1—O1^xiii	3.282 (11)	Cs1—O2^l	3.15 (3)
Cs1—O1^xiv	3.282 (11)	Cs1—O2^li	3.15 (3)
Cs1—O1^xv	3.282 (11)	Cs1—O2^lii	3.15 (3)
Cs1—O1^xvi	3.282 (11)	Cs1—O2^liii	3.15 (3)
Cs1—O1^xvii	3.282 (11)	Cs1—O2^liv	3.15 (3)
Cs1—O1^xviii	3.282 (11)	Cs1—O2^lv	3.15 (3)
Cs1—O1^xix	3.282 (11)	Cs1—O2^lvi	3.15 (3)
Cs1—O1^xx	3.282 (11)	Cs1—O2^lvii	3.15 (3)
Cs1—O1^xxi	3.282 (11)	Cs1—O2^lviii	3.15 (3)
Cs1—O1^xxii	3.282 (11)	Cs1—O2^lix	3.15 (3)
Cs1—O1^xxiii	3.282 (11)	Cs1—O2^lx	3.15 (3)
Cs1—O1^xxiv	3.282 (11)	Cs1—O2^lxi	3.15 (3)
Cs1—O1^xxv	3.282 (11)	Cs1—O2^lxii	3.15 (3)
Cs1—O2^xxvi	3.15 (3)	Cs1—O2^lxiii	3.15 (3)
Cs1—O2^xxvii	3.15 (3)	Cs1—O2^lxiv	3.15 (3)
Cs1—O2^xxviii	3.15 (3)	Cs1—O2^lxv	3.15 (3)
Cs1—O2ⁱ	3.15 (3)	Cs1—O2^lxvi	3.15 (3)
Cs1—O2^xxix	3.15 (3)	Cs1—O2^lxvii	3.15 (3)
Cs1—O2^xxx	3.15 (3)	Cs1—O2^lxviii	3.15 (3)
Cs1—O2^xxxi	3.15 (3)	Cs1—O2^lxix	3.15 (3)
Cs1—O2^xxxii	3.15 (3)	Cs1—O2^lxx	3.15 (3)
Cs1—O2^xxxiii	3.15 (3)	Cs1—O2^lxxi	3.15 (3)
Cs1—O2^xxxiv	3.15 (3)	Cs1—O2^lxxii	3.15 (3)
Cs1—O2^xxxv	3.15 (3)

O1—N1—O2	119 (3)	O1^xxiii—Cs1—O2^lxix	89.9 (9)
O1—N1—O2ⁱ	119 (3)	O1^xxiii—Cs1—O2^lxx	71.0 (8)
O2—N1—O2ⁱ	123 (5)	O1^xxiii—Cs1—O2^lxxi	60.3 (9)
O1ⁱⁱ—Cs1—O1ⁱⁱⁱ	87.1 (3)	O1^xxiii—Cs1—O2^lxxii	35.0 (9)
O1ⁱⁱ—Cs1—O1^iv	87.1 (3)	O1^xxiv—Cs1—O1^xxv	87.1 (3)
O1ⁱⁱ—Cs1—O1^v	154.0 (11)	O1^xxiv—Cs1—O2^xxvi	145.0 (9)
O1ⁱⁱ—Cs1—O1^vi	26.0 (11)	O1^xxiv—Cs1—O2^xxvii	119.7 (9)
O1ⁱⁱ—Cs1—O1^vii	92.9 (3)	O1^xxiv—Cs1—O2^xxviii	109.0 (8)
O1ⁱⁱ—Cs1—O1^viii	92.9 (3)	O1^xxiv—Cs1—O2ⁱ	90.1 (9)
O1ⁱⁱ—Cs1—O1^ix	180	O1^xxiv—Cs1—O2^xxix	60.3 (9)
O1ⁱⁱ—Cs1—O1^xi	61.7 (9)	O1^xxiv—Cs1—O2^xxx	35.0 (9)
O1ⁱⁱ—Cs1—O1^xii	99.5 (9)	O1^xxiv—Cs1—O2^xxxi	89.9 (9)
O1ⁱⁱ—Cs1—O1^xiii	118.3 (9)	O1^xxiv—Cs1—O2^xxxii	71.0 (8)
O1ⁱⁱ—Cs1—O1^xiv	61.7 (9)	O1^xxiv—Cs1—O2^xxxiii	34.4 (10)
O1ⁱⁱ—Cs1—O1^xv	80.5 (9)	O1^xxiv—Cs1—O2^xxxiv	99.5 (7)
O1ⁱⁱ—Cs1—O1^xvi	118.3 (9)	O1^xxiv—Cs1—O2^xxxvi	90.2 (6)
O1ⁱⁱ—Cs1—O1^xvii	141.7 (10)	O1^xxiv—Cs1—O2^xxxvii	80.5 (7)
O1ⁱⁱ—Cs1—O1^xix	61.7 (9)	O1^xxiv—Cs1—O2^xxxviii	145.6 (10)
O1ⁱⁱ—Cs1—O1^xx	99.5 (9)	O1^xxiv—Cs1—O2^xxxix	89.8 (6)
O1ⁱⁱ—Cs1—O1^xxi	118.3 (9)	O1^xxiv—Cs1—O2^xl	170.5 (9)
O1ⁱⁱ—Cs1—O1^xxii	61.7 (9)	O1^xxiv—Cs1—O2^xli	96.6 (7)
O1ⁱⁱ—Cs1—O1^xxiii	80.5 (9)	O1^xxiv—Cs1—O2^xlii	28.8 (9)
O1ⁱⁱ—Cs1—O1^xxiv	118.3 (9)	O1^xxiv—Cs1—O2^xliii	127.5 (10)
O1ⁱⁱ—Cs1—O1^xxv	141.7 (10)	O1^xxiv—Cs1—O2^xliv	67.5 (6)
O1ⁱⁱ—Cs1—O2^xxvii	112.5 (6)	O1^xxiv—Cs1—O2^xlv	151.2 (9)
O1ⁱⁱ—Cs1—O2^xxviii	83.4 (7)	O1^xxiv—Cs1—O2^xlvi	83.4 (7)
O1ⁱⁱ—Cs1—O2ⁱ	151.2 (9)	O1^xxiv—Cs1—O2^xlvii	112.5 (6)
O1ⁱⁱ—Cs1—O2^xxx	127.5 (10)	O1^xxiv—Cs1—O2^xlviii	52.5 (10)
O1ⁱⁱ—Cs1—O2^xxxi	28.8 (9)	O1^xxiv—Cs1—O2^xlix	99.5 (7)
O1ⁱⁱ—Cs1—O2^xxxii	96.6 (7)	O1^xxiv—Cs1—O2^l	34.4 (10)
O1ⁱⁱ—Cs1—O2^xxxiii	90.1 (9)	O1^xxiv—Cs1—O2^li	90.2 (6)
O1ⁱⁱ—Cs1—O2^xxxiv	109.0 (8)	O1^xxiv—Cs1—O2^liii	145.6 (10)
O1ⁱⁱ—Cs1—O2^xxxv	119.7 (9)	O1^xxiv—Cs1—O2^liv	80.5 (7)
O1ⁱⁱ—Cs1—O2^xxxvi	145.0 (9)	O1^xxiv—Cs1—O2^lv	170.5 (9)
O1ⁱⁱ—Cs1—O2^xxxviii	89.9 (9)	O1^xxiv—Cs1—O2^lvi	89.8 (6)
O1ⁱⁱ—Cs1—O2^xlii	145.6 (10)	O1^xxiv—Cs1—O2^lvii	67.5 (6)
O1ⁱⁱ—Cs1—O2^xliii	89.8 (6)	O1^xxiv—Cs1—O2^lviii	127.5 (10)
O1ⁱⁱ—Cs1—O2^xliv	170.5 (9)	O1^xxiv—Cs1—O2^lx	96.6 (7)
O1ⁱⁱ—Cs1—O2^xlv	34.4 (10)	O1^xxiv—Cs1—O2^lxi	52.5 (10)
O1ⁱⁱ—Cs1—O2^xlvi	99.5 (7)	O1^xxiv—Cs1—O2^lxii	112.5 (6)
O1ⁱⁱ—Cs1—O2^xlviii	90.2 (6)	O1^xxiv—Cs1—O2^lxiii	83.4 (7)
O1ⁱⁱ—Cs1—O2^l	96.6 (7)	O1^xxiv—Cs1—O2^lxiv	151.2 (9)
O1ⁱⁱ—Cs1—O2^li	67.5 (6)	O1^xxiv—Cs1—O2^lxv	89.9 (9)
O1ⁱⁱ—Cs1—O2^lii	127.5 (10)	O1^xxiv—Cs1—O2^lxvi	71.0 (8)
O1ⁱⁱ—Cs1—O2^liii	83.4 (7)	O1^xxiv—Cs1—O2^lxvii	60.3 (9)
O1ⁱⁱ—Cs1—O2^liv	151.2 (9)	O1^xxiv—Cs1—O2^lxix	109.0 (8)
O1ⁱⁱ—Cs1—O2^lvi	112.5 (6)	O1^xxiv—Cs1—O2^lxx	90.1 (9)
O1ⁱⁱ—Cs1—O2^lviii	109.0 (8)	O1^xxiv—Cs1—O2^lxxi	145.0 (9)
O1ⁱⁱ—Cs1—O2^lix	119.7 (9)	O1^xxiv—Cs1—O2^lxxii	119.7 (9)
O1ⁱⁱ—Cs1—O2^lx	145.0 (9)	O1^xxv—Cs1—O2^xxvi	89.9 (9)
O1ⁱⁱ—Cs1—O2^lxv	89.8 (6)	O1^xxv—Cs1—O2^xxvii	71.0 (8)
O1ⁱⁱ—Cs1—O2^lxvi	170.5 (9)	O1^xxv—Cs1—O2^xxviii	60.3 (9)
O1ⁱⁱ—Cs1—O2^lxvii	80.5 (7)	O1^xxv—Cs1—O2^xxix	109.0 (8)
O1ⁱⁱ—Cs1—O2^lxviii	145.6 (10)	O1^xxv—Cs1—O2^xxx	90.1 (9)
O1ⁱⁱ—Cs1—O2^lxix	9.5 (9)	O1^xxv—Cs1—O2^xxxi	145.0 (9)
O1ⁱⁱ—Cs1—O2^lxx	90.2 (6)	O1^xxv—Cs1—O2^xxxii	119.7 (9)
O1ⁱⁱ—Cs1—O2^lxxi	34.4 (10)	O1^xxv—Cs1—O2^xxxiii	99.5 (7)
O1ⁱⁱ—Cs1—O2^lxxii	99.5 (7)	O1^xxv—Cs1—O2^xxxiv	34.4 (10)
O1ⁱⁱⁱ—Cs1—O1^iv	154.0 (11)	O1^xxv—Cs1—O2^xxxv	90.2 (6)
O1ⁱⁱⁱ—Cs1—O1^v	87.1 (3)	O1^xxv—Cs1—O2^xxxvii	145.6 (10)
O1ⁱⁱⁱ—Cs1—O1^vi	92.9 (3)	O1^xxv—Cs1—O2^xxxviii	80.5 (7)
O1ⁱⁱⁱ—Cs1—O1^viii	180	O1^xxv—Cs1—O2^xxxix	170.5 (9)
O1ⁱⁱⁱ—Cs1—O1^ix	92.9 (3)	O1^xxv—Cs1—O2^xl	89.8 (6)
O1ⁱⁱⁱ—Cs1—O1^x	99.5 (9)	O1^xxv—Cs1—O2^xli	127.5 (10)
O1ⁱⁱⁱ—Cs1—O1^xi	118.3 (9)	O1^xxv—Cs1—O2^xlii	67.5 (6)
O1ⁱⁱⁱ—Cs1—O1^xiv	118.3 (9)	O1^xxv—Cs1—O2^xliii	96.6 (7)
O1ⁱⁱⁱ—Cs1—O1^xv	141.7 (10)	O1^xxv—Cs1—O2^xliv	28.8 (9)
O1ⁱⁱⁱ—Cs1—O1^xvi	61.7 (9)	O1^xxv—Cs1—O2^xlv	112.5 (6)
O1ⁱⁱⁱ—Cs1—O1^xvii	80.5 (9)	O1^xxv—Cs1—O2^xlvi	52.5 (10)
O1ⁱⁱⁱ—Cs1—O1^xviii	61.7 (9)	O1^xxv—Cs1—O2^xlvii	151.2 (9)
O1ⁱⁱⁱ—Cs1—O1^xix	80.5 (9)	O1^xxv—Cs1—O2^xlviii	83.4 (7)
O1ⁱⁱⁱ—Cs1—O1^xx	118.3 (9)	O1^xxv—Cs1—O2^xlix	170.5 (9)
O1ⁱⁱⁱ—Cs1—O1^xxi	141.7 (10)	O1^xxv—Cs1—O2^l	89.8 (6)
O1ⁱⁱⁱ—Cs1—O1^xxiii	61.7 (9)	O1^xxv—Cs1—O2^li	145.6 (10)
O1ⁱⁱⁱ—Cs1—O1^xxiv	99.5 (9)	O1^xxv—Cs1—O2^lii	80.5 (7)
O1ⁱⁱⁱ—Cs1—O1^xxv	118.3 (9)	O1^xxv—Cs1—O2^liii	90.2 (6)
O1ⁱⁱⁱ—Cs1—O2^xxvi	112.5 (6)	O1^xxv—Cs1—O2^liv	9.5 (9)
O1ⁱⁱⁱ—Cs1—O2^xxvii	52.5 (10)	O1^xxv—Cs1—O2^lv	99.5 (7)
O1ⁱⁱⁱ—Cs1—O2^xxviii	151.2 (9)	O1^xxv—Cs1—O2^lvi	34.4 (10)
O1ⁱⁱⁱ—Cs1—O2ⁱ	83.4 (7)	O1^xxv—Cs1—O2^lvii	127.5 (10)
O1ⁱⁱⁱ—Cs1—O2^xxix	127.5 (10)	O1^xxv—Cs1—O2^lviii	67.5 (6)
O1ⁱⁱⁱ—Cs1—O2^xxxi	96.6 (7)	O1^xxv—Cs1—O2^lix	96.6 (7)
O1ⁱⁱⁱ—Cs1—O2^xxxiii	119.7 (9)	O1^xxv—Cs1—O2^lx	28.8 (9)
O1ⁱⁱⁱ—Cs1—O2^xxxiv	145.0 (9)	O1^xxv—Cs1—O2^lxi	112.5 (6)
O1ⁱⁱⁱ—Cs1—O2^xxxv	90.1 (9)	O1^xxv—Cs1—O2^lxii	52.5 (10)
O1ⁱⁱⁱ—Cs1—O2^xxxvi	109.0 (8)	O1^xxv—Cs1—O2^lxiii	151.2 (9)
O1ⁱⁱⁱ—Cs1—O2^xxxviii	60.3 (9)	O1^xxv—Cs1—O2^lxiv	83.4 (7)
O1ⁱⁱⁱ—Cs1—O2^xxxix	71.0 (8)	O1^xxv—Cs1—O2^lxv	60.3 (9)
O1ⁱⁱⁱ—Cs1—O2^xl	89.9 (9)	O1^xxv—Cs1—O2^lxvii	89.9 (9)
O1ⁱⁱⁱ—Cs1—O2^xli	9.5 (9)	O1^xxv—Cs1—O2^lxviii	71.0 (8)
O1ⁱⁱⁱ—Cs1—O2^xlii	90.2 (6)	O1^xxv—Cs1—O2^lxix	145.0 (9)
O1ⁱⁱⁱ—Cs1—O2^xliv	99.5 (7)	O1^xxv—Cs1—O2^lxx	119.7 (9)
O1ⁱⁱⁱ—Cs1—O2^xlv	89.8 (6)	O1^xxv—Cs1—O2^lxxi	109.0 (8)
O1ⁱⁱⁱ—Cs1—O2^xlvi	170.5 (9)	O1^xxv—Cs1—O2^lxxii	90.1 (9)
O1ⁱⁱⁱ—Cs1—O2^xlvii	80.5 (7)	O2^xxvi—Cs1—O2^xxvii	91.9 (7)
O1ⁱⁱⁱ—Cs1—O2^xlviii	145.6 (10)	O2^xxvi—Cs1—O2^xxviii	42.0 (7)
O1ⁱⁱⁱ—Cs1—O2^xlix	67.5 (6)	O2^xxvi—Cs1—O2ⁱ	106.9 (9)
O1ⁱⁱⁱ—Cs1—O2^l	127.5 (10)	O2^xxvi—Cs1—O2^xxix	88.1 (7)
O1ⁱⁱⁱ—Cs1—O2^lii	96.6 (7)	O2^xxvi—Cs1—O2^xxx	180
O1ⁱⁱⁱ—Cs1—O2^liii	52.5 (10)	O2^xxvi—Cs1—O2^xxxi	73.1 (9)
O1ⁱⁱⁱ—Cs1—O2^liv	112.5 (6)	O2^xxvi—Cs1—O2^xxxii	138.0 (7)
O1ⁱⁱⁱ—Cs1—O2^lv	83.4 (7)	O2^xxvi—Cs1—O2^xxxiii	112.6 (7)
O1ⁱⁱⁱ—Cs1—O2^lvi	151.2 (9)	O2^xxvi—Cs1—O2^xxxiv	61.8 (9)
O1ⁱⁱⁱ—Cs1—O2^lviii	60.3 (9)	O2^xxvi—Cs1—O2^xxxv	154.1 (7)
O1ⁱⁱⁱ—Cs1—O2^lix	71.0 (8)	O2^xxvi—Cs1—O2^xxxvi	92.5 (8)
O1ⁱⁱⁱ—Cs1—O2^lx	89.9 (9)	O2^xxvi—Cs1—O2^xxxvii	118.2 (9)
O1ⁱⁱⁱ—Cs1—O2^lxi	119.7 (9)	O2^xxvi—Cs1—O2^xxxviii	67.4 (7)
O1ⁱⁱⁱ—Cs1—O2^lxii	145.0 (9)	O2^xxvi—Cs1—O2^xxxix	87.5 (8)
O1ⁱⁱⁱ—Cs1—O2^lxiii	90.1 (9)	O2^xxvi—Cs1—O2^xli	112.6 (7)
O1ⁱⁱⁱ—Cs1—O2^lxiv	109.0 (8)	O2^xxvi—Cs1—O2^xlii	154.1 (7)
O1ⁱⁱⁱ—Cs1—O2^lxv	170.5 (9)	O2^xxvi—Cs1—O2^xliii	87.5 (8)
O1ⁱⁱⁱ—Cs1—O2^lxvi	89.8 (6)	O2^xxvi—Cs1—O2^xliv	118.2 (9)
O1ⁱⁱⁱ—Cs1—O2^lxvii	145.6 (10)	O2^xxvi—Cs1—O2^xlv	25.9 (7)
O1ⁱⁱⁱ—Cs1—O2^lxviii	80.5 (7)	O2^xxvi—Cs1—O2^xlvi	67.4 (7)
O1ⁱⁱⁱ—Cs1—O2^lxix	90.2 (6)	O2^xxvi—Cs1—O2^xlvii	61.8 (9)
O1ⁱⁱⁱ—Cs1—O2^lxxi	99.5 (7)	O2^xxvi—Cs1—O2^xlviii	92.5 (8)
O1^iv—Cs1—O1^v	87.1 (3)	O2^xxvi—Cs1—O2^xlix	80.8 (9)
O1^iv—Cs1—O1^vi	92.9 (3)	O2^xxvi—Cs1—O2^l	110.8 (7)
O1^iv—Cs1—O1^vii	180	O2^xxvi—Cs1—O2^li	110.8 (7)
O1^iv—Cs1—O1^ix	92.9 (3)	O2^xxvi—Cs1—O2^lii	150.5 (6)
O1^iv—Cs1—O1^x	61.7 (9)	O2^xxvi—Cs1—O2^liii	69.2 (7)
O1^iv—Cs1—O1^xi	80.5 (9)	O2^xxvi—Cs1—O2^liv	99.2 (9)
O1^iv—Cs1—O1^xii	118.3 (9)	O2^xxvi—Cs1—O2^lv	29.5 (6)
O1^iv—Cs1—O1^xiii	141.7 (10)	O2^xxvi—Cs1—O2^lvi	69.2 (7)
O1^iv—Cs1—O1^xv	61.7 (9)	O2^xxvi—Cs1—O2^lvii	136.7 (8)
O1^iv—Cs1—O1^xvi	99.5 (9)	O2^xxvi—Cs1—O2^lviii	82.6 (9)
O1^iv—Cs1—O1^xvii	118.3 (9)	O2^xxvi—Cs1—O2^lix	170.0 (9)
O1^iv—Cs1—O1^xviii	99.5 (9)	O2^xxvi—Cs1—O2^lx	97.4 (9)
O1^iv—Cs1—O1^xix	118.3 (9)	O2^xxvi—Cs1—O2^lxi	97.4 (9)
O1^iv—Cs1—O1^xxi	61.7 (9)	O2^xxvi—Cs1—O2^lxii	43.3 (8)
O1^iv—Cs1—O1^xxii	118.3 (9)	O2^xxvi—Cs1—O2^lxiii	82.6 (9)
O1^iv—Cs1—O1^xxiii	141.7 (10)	O2^xxvi—Cs1—O2^lxiv	10.0 (9)
O1^iv—Cs1—O1^xxiv	61.7 (9)	O2^xxvi—Cs1—O2^lxv	58.9 (8)
O1^iv—Cs1—O1^xxv	80.5 (9)	O2^xxvi—Cs1—O2^lxvi	121.1 (8)
O1^iv—Cs1—O2^xxvi	83.4 (7)	O2^xxvi—Cs1—O2^lxvii	84.9 (6)
O1^iv—Cs1—O2^xxvii	151.2 (9)	O2^xxvi—Cs1—O2^lxviii	160.7 (9)
O1^iv—Cs1—O2ⁱ	112.5 (6)	O2^xxvi—Cs1—O2^lxix	58.9 (8)
O1^iv—Cs1—O2^xxx	96.6 (7)	O2^xxvi—Cs1—O2^lxx	121.1 (8)
O1^iv—Cs1—O2^xxxi	67.5 (6)	O2^xxvi—Cs1—O2^lxxi	19.3 (9)
O1^iv—Cs1—O2^xxxii	127.5 (10)	O2^xxvi—Cs1—O2^lxxii	95.1 (6)
O1^iv—Cs1—O2^xxxiii	35.0 (9)	O2^xxvii—Cs1—O2^xxviii	106.9 (9)
O1^iv—Cs1—O2^xxxiv	60.3 (9)	O2^xxvii—Cs1—O2ⁱ	42.0 (7)
O1^iv—Cs1—O2^xxxv	71.0 (8)	O2^xxvii—Cs1—O2^xxix	180
O1^iv—Cs1—O2^xxxvi	89.9 (9)	O2^xxvii—Cs1—O2^xxx	88.1 (7)
O1^iv—Cs1—O2^xxxvii	119.7 (9)	O2^xxvii—Cs1—O2^xxxi	138.0 (7)
O1^iv—Cs1—O2^xxxviii	145.0 (9)	O2^xxvii—Cs1—O2^xxxii	73.1 (9)
O1^iv—Cs1—O2^xxxix	90.1 (9)	O2^xxvii—Cs1—O2^xxxiii	154.1 (7)
O1^iv—Cs1—O2^xl	109.0 (8)	O2^xxvii—Cs1—O2^xxxiv	92.5 (8)
O1^iv—Cs1—O2^xli	145.6 (10)	O2^xxvii—Cs1—O2^xxxv	112.6 (7)
O1^iv—Cs1—O2^xlii	80.5 (7)	O2^xxvii—Cs1—O2^xxxvi	61.8 (9)
O1^iv—Cs1—O2^xliii	170.5 (9)	O2^xxvii—Cs1—O2^xxxvii	87.5 (8)
O1^iv—Cs1—O2^xliv	89.8 (6)	O2^xxvii—Cs1—O2^xxxviii	25.9 (7)
O1^iv—Cs1—O2^xlv	99.5 (7)	O2^xxvii—Cs1—O2^xxxix	118.2 (9)
O1^iv—Cs1—O2^xlvii	90.2 (6)	O2^xxvii—Cs1—O2^xl	67.4 (7)
O1^iv—Cs1—O2^xlix	96.6 (7)	O2^xxvii—Cs1—O2^xli	61.8 (9)
O1^iv—Cs1—O2^li	127.5 (10)	O2^xxvii—Cs1—O2^xlii	92.5 (8)
O1^iv—Cs1—O2^liii	151.2 (9)	O2^xxvii—Cs1—O2^xliii	25.9 (7)
O1^iv—Cs1—O2^liv	83.4 (7)	O2^xxvii—Cs1—O2^xliv	67.4 (7)
O1^iv—Cs1—O2^lv	112.5 (6)	O2^xxvii—Cs1—O2^xlv	87.5 (8)
O1^iv—Cs1—O2^lvi	52.5 (10)	O2^xxvii—Cs1—O2^xlvi	118.2 (9)
O1^iv—Cs1—O2^lvii	119.7 (9)	O2^xxvii—Cs1—O2^xlvii	112.6 (7)
O1^iv—Cs1—O2^lviii	145.0 (9)	O2^xxvii—Cs1—O2^xlviii	154.1 (7)
O1^iv—Cs1—O2^lix	90.1 (9)	O2^xxvii—Cs1—O2^xlix	110.8 (7)
O1^iv—Cs1—O2^lx	109.0 (8)	O2^xxvii—Cs1—O2^l	150.5 (6)
O1^iv—Cs1—O2^lxii	60.3 (9)	O2^xxvii—Cs1—O2^li	80.8 (9)
O1^iv—Cs1—O2^lxiii	71.0 (8)	O2^xxvii—Cs1—O2^lii	110.8 (7)
O1^iv—Cs1—O2^lxiv	89.9 (9)	O2^xxvii—Cs1—O2^liii	29.5 (6)
O1^iv—Cs1—O2^lxvi	99.5 (7)	O2^xxvii—Cs1—O2^liv	69.2 (7)
O1^iv—Cs1—O2^lxvii	9.5 (9)	O2^xxvii—Cs1—O2^lv	69.2 (7)
O1^iv—Cs1—O2^lxviii	90.2 (6)	O2^xxvii—Cs1—O2^lvi	99.2 (9)
O1^iv—Cs1—O2^lxix	80.5 (7)	O2^xxvii—Cs1—O2^lvii	82.6 (9)
O1^iv—Cs1—O2^lxx	145.6 (10)	O2^xxvii—Cs1—O2^lviii	10.0 (9)
O1^iv—Cs1—O2^lxxi	89.8 (6)	O2^xxvii—Cs1—O2^lix	97.4 (9)
O1^iv—Cs1—O2^lxxii	170.5 (9)	O2^xxvii—Cs1—O2^lx	43.3 (8)
O1^v—Cs1—O1^vi	180	O2^xxvii—Cs1—O2^lxi	170.0 (9)
O1^v—Cs1—O1^vii	92.9 (3)	O2^xxvii—Cs1—O2^lxii	97.4 (9)
O1^v—Cs1—O1^viii	92.9 (3)	O2^xxvii—Cs1—O2^lxiii	136.7 (8)
O1^v—Cs1—O1^ix	26.0 (11)	O2^xxvii—Cs1—O2^lxiv	82.6 (9)
O1^v—Cs1—O1^x	118.3 (9)	O2^xxvii—Cs1—O2^lxv	121.1 (8)
O1^v—Cs1—O1^xi	141.7 (10)	O2^xxvii—Cs1—O2^lxvi	58.9 (8)
O1^v—Cs1—O1^xii	61.7 (9)	O2^xxvii—Cs1—O2^lxvii	160.7 (9)
O1^v—Cs1—O1^xiii	80.5 (9)	O2^xxvii—Cs1—O2^lxviii	84.9 (6)
O1^v—Cs1—O1^xiv	99.5 (9)	O2^xxvii—Cs1—O2^lxix	121.1 (8)
O1^v—Cs1—O1^xv	118.3 (9)	O2^xxvii—Cs1—O2^lxx	58.9 (8)
O1^v—Cs1—O1^xvi	38.3 (10)	O2^xxvii—Cs1—O2^lxxi	95.1 (6)
O1^v—Cs1—O1^xvii	61.7 (9)	O2^xxvii—Cs1—O2^lxxii	19.3 (9)
O1^v—Cs1—O1^xviii	118.3 (9)	O2^xxviii—Cs1—O2ⁱ	91.9 (7)
O1^v—Cs1—O1^xix	141.7 (10)	O2^xxviii—Cs1—O2^xxix	73.1 (9)
O1^v—Cs1—O1^xx	61.7 (9)	O2^xxviii—Cs1—O2^xxx	138.0 (7)
O1^v—Cs1—O1^xxi	80.5 (9)	O2^xxviii—Cs1—O2^xxxi	88.1 (7)
O1^v—Cs1—O1^xxii	99.5 (9)	O2^xxviii—Cs1—O2^xxxii	180
O1^v—Cs1—O1^xxiii	118.3 (9)	O2^xxviii—Cs1—O2^xxxiii	87.5 (8)
O1^v—Cs1—O1^xxiv	38.3 (10)	O2^xxviii—Cs1—O2^xxxiv	25.9 (7)
O1^v—Cs1—O1^xxv	61.7 (9)	O2^xxviii—Cs1—O2^xxxv	118.2 (9)
O1^v—Cs1—O2^xxvi	151.2 (9)	O2^xxviii—Cs1—O2^xxxvi	67.4 (7)
O1^v—Cs1—O2^xxvii	83.4 (7)	O2^xxviii—Cs1—O2^xxxvii	154.1 (7)
O1^v—Cs1—O2^xxviii	112.5 (6)	O2^xxviii—Cs1—O2^xxxviii	92.5 (8)
O1^v—Cs1—O2ⁱ	52.5 (10)	O2^xxviii—Cs1—O2^xxxix	112.6 (7)
O1^v—Cs1—O2^xxix	96.6 (7)	O2^xxviii—Cs1—O2^xl	61.8 (9)
O1^v—Cs1—O2^xxx	28.8 (9)	O2^xxviii—Cs1—O2^xli	154.1 (7)
O1^v—Cs1—O2^xxxi	127.5 (10)	O2^xxviii—Cs1—O2^xlii	112.6 (7)
O1^v—Cs1—O2^xxxii	67.5 (6)	O2^xxviii—Cs1—O2^xliii	118.2 (9)
O1^v—Cs1—O2^xxxiii	71.0 (8)	O2^xxviii—Cs1—O2^xliv	87.5 (8)
O1^v—Cs1—O2^xxxiv	89.9 (9)	O2^xxviii—Cs1—O2^xlv	67.4 (7)
O1^v—Cs1—O2^xxxv	35.0 (9)	O2^xxviii—Cs1—O2^xlvi	25.9 (7)
O1^v—Cs1—O2^xxxvi	60.3 (9)	O2^xxviii—Cs1—O2^xlvii	92.5 (8)
O1^v—Cs1—O2^xxxvii	90.1 (9)	O2^xxviii—Cs1—O2^xlviii	61.8 (9)
O1^v—Cs1—O2^xxxviii	109.0 (8)	O2^xxviii—Cs1—O2^xlix	110.8 (7)
O1^v—Cs1—O2^xxxix	119.7 (9)	O2^xxviii—Cs1—O2^l	80.8 (9)
O1^v—Cs1—O2^xl	145.0 (9)	O2^xxviii—Cs1—O2^li	150.5 (6)
O1^v—Cs1—O2^xli	90.2 (6)	O2^xxviii—Cs1—O2^lii	110.8 (7)
O1^v—Cs1—O2^xlii	9.5 (9)	O2^xxviii—Cs1—O2^liii	99.2 (9)
O1^v—Cs1—O2^xliii	99.5 (7)	O2^xxviii—Cs1—O2^liv	69.2 (7)
O1^v—Cs1—O2^xliv	34.4 (10)	O2^xxviii—Cs1—O2^lv	69.2 (7)
O1^v—Cs1—O2^xlv	170.5 (9)	O2^xxviii—Cs1—O2^lvi	29.5 (6)
O1^v—Cs1—O2^xlvi	89.8 (6)	O2^xxviii—Cs1—O2^lvii	170.0 (9)
O1^v—Cs1—O2^xlvii	145.6 (10)	O2^xxviii—Cs1—O2^lviii	97.4 (9)
O1^v—Cs1—O2^xlviii	80.5 (7)	O2^xxviii—Cs1—O2^lix	136.7 (8)
O1^v—Cs1—O2^xlix	127.5 (10)	O2^xxviii—Cs1—O2^lx	82.6 (9)
O1^v—Cs1—O2^l	67.5 (6)	O2^xxviii—Cs1—O2^lxi	82.6 (9)
O1^v—Cs1—O2^li	96.6 (7)	O2^xxviii—Cs1—O2^lxiii	97.4 (9)
O1^v—Cs1—O2^lii	28.8 (9)	O2^xxviii—Cs1—O2^lxiv	43.3 (8)
O1^v—Cs1—O2^liii	112.5 (6)	O2^xxviii—Cs1—O2^lxv	19.3 (9)
O1^v—Cs1—O2^liv	52.5 (10)	O2^xxviii—Cs1—O2^lxvi	95.1 (6)
O1^v—Cs1—O2^lv	151.2 (9)	O2^xxviii—Cs1—O2^lxvii	58.9 (8)
O1^v—Cs1—O2^lvi	83.4 (7)	O2^xxviii—Cs1—O2^lxviii	121.1 (8)
O1^v—Cs1—O2^lvii	71.0 (8)	O2^xxviii—Cs1—O2^lxix	84.9 (6)
O1^v—Cs1—O2^lviii	89.9 (9)	O2^xxviii—Cs1—O2^lxx	160.7 (9)
O1^v—Cs1—O2^lix	35.0 (9)	O2^xxviii—Cs1—O2^lxxi	58.9 (8)
O1^v—Cs1—O2^lx	60.3 (9)	O2^xxviii—Cs1—O2^lxxii	121.1 (8)
O1^v—Cs1—O2^lxi	90.1 (9)	O2ⁱ—Cs1—O2^xxix	138.0 (7)
O1^v—Cs1—O2^lxii	109.0 (8)	O2ⁱ—Cs1—O2^xxx	73.1 (9)
O1^v—Cs1—O2^lxiii	119.7 (9)	O2ⁱ—Cs1—O2^xxxi	180
O1^v—Cs1—O2^lxiv	145.0 (9)	O2ⁱ—Cs1—O2^xxxii	88.1 (7)
O1^v—Cs1—O2^lxv	99.5 (7)	O2ⁱ—Cs1—O2^xxxiii	118.2 (9)
O1^v—Cs1—O2^lxvi	34.4 (10)	O2ⁱ—Cs1—O2^xxxiv	67.4 (7)
O1^v—Cs1—O2^lxvii	90.2 (6)	O2ⁱ—Cs1—O2^xxxv	87.5 (8)
O1^v—Cs1—O2^lxix	145.6 (10)	O2ⁱ—Cs1—O2^xxxvi	25.9 (7)
O1^v—Cs1—O2^lxx	80.5 (7)	O2ⁱ—Cs1—O2^xxxvii	112.6 (7)
O1^v—Cs1—O2^lxxi	170.5 (9)	O2ⁱ—Cs1—O2^xxxviii	61.8 (9)
O1^v—Cs1—O2^lxxii	89.8 (6)	O2ⁱ—Cs1—O2^xxxix	154.1 (7)
O1^vi—Cs1—O1^vii	87.1 (3)	O2ⁱ—Cs1—O2^xl	92.5 (8)
O1^vi—Cs1—O1^viii	87.1 (3)	O2ⁱ—Cs1—O2^xli	92.5 (8)
O1^vi—Cs1—O1^ix	154.0 (11)	O2ⁱ—Cs1—O2^xlii	61.8 (9)
O1^vi—Cs1—O1^x	61.7 (9)	O2ⁱ—Cs1—O2^xliii	67.4 (7)
O1^vi—Cs1—O1^xi	38.3 (10)	O2ⁱ—Cs1—O2^xliv	25.9 (7)
O1^vi—Cs1—O1^xii	118.3 (9)	O2ⁱ—Cs1—O2^xlv	118.2 (9)
O1^vi—Cs1—O1^xiii	99.5 (9)	O2ⁱ—Cs1—O2^xlvi	87.5 (8)
O1^vi—Cs1—O1^xiv	80.5 (9)	O2ⁱ—Cs1—O2^xlvii	154.1 (7)
O1^vi—Cs1—O1^xv	61.7 (9)	O2ⁱ—Cs1—O2^xlviii	112.6 (7)
O1^vi—Cs1—O1^xvi	141.7 (10)	O2ⁱ—Cs1—O2^xlix	150.5 (6)
O1^vi—Cs1—O1^xvii	118.3 (9)	O2ⁱ—Cs1—O2^l	110.8 (7)
O1^vi—Cs1—O1^xviii	61.7 (9)	O2ⁱ—Cs1—O2^li	110.8 (7)
O1^vi—Cs1—O1^xix	38.3 (10)	O2ⁱ—Cs1—O2^lii	80.8 (9)
O1^vi—Cs1—O1^xx	118.3 (9)	O2ⁱ—Cs1—O2^liii	69.2 (7)
O1^vi—Cs1—O1^xxi	99.5 (9)	O2ⁱ—Cs1—O2^liv	29.5 (6)
O1^vi—Cs1—O1^xxii	80.5 (9)	O2ⁱ—Cs1—O2^lv	99.2 (9)
O1^vi—Cs1—O1^xxiii	61.7 (9)	O2ⁱ—Cs1—O2^lvi	69.2 (7)
O1^vi—Cs1—O1^xxiv	141.7 (10)	O2ⁱ—Cs1—O2^lvii	97.4 (9)
O1^vi—Cs1—O1^xxv	118.3 (9)	O2ⁱ—Cs1—O2^lviii	43.3 (8)
O1^vi—Cs1—O2^xxvi	28.8 (9)	O2ⁱ—Cs1—O2^lix	82.6 (9)
O1^vi—Cs1—O2^xxvii	96.6 (7)	O2ⁱ—Cs1—O2^lx	10.0 (9)
O1^vi—Cs1—O2^xxviii	67.5 (6)	O2ⁱ—Cs1—O2^lxi	136.7 (8)
O1^vi—Cs1—O2ⁱ	127.5 (10)	O2ⁱ—Cs1—O2^lxii	82.6 (9)
O1^vi—Cs1—O2^xxix	83.4 (7)	O2ⁱ—Cs1—O2^lxiii	170.0 (9)
O1^vi—Cs1—O2^xxx	151.2 (9)	O2ⁱ—Cs1—O2^lxiv	97.4 (9)
O1^vi—Cs1—O2^xxxi	52.5 (10)	O2ⁱ—Cs1—O2^lxv	95.1 (6)
O1^vi—Cs1—O2^xxxii	112.5 (6)	O2ⁱ—Cs1—O2^lxvi	19.3 (9)
O1^vi—Cs1—O2^xxxiii	109.0 (8)	O2ⁱ—Cs1—O2^lxvii	121.1 (8)
O1^vi—Cs1—O2^xxxiv	90.1 (9)	O2ⁱ—Cs1—O2^lxviii	58.9 (8)
O1^vi—Cs1—O2^xxxv	145.0 (9)	O2ⁱ—Cs1—O2^lxix	160.7 (9)
O1^vi—Cs1—O2^xxxvi	119.7 (9)	O2ⁱ—Cs1—O2^lxx	84.9 (6)
O1^vi—Cs1—O2^xxxvii	89.9 (9)	O2ⁱ—Cs1—O2^lxxi	121.1 (8)
O1^vi—Cs1—O2^xxxviii	71.0 (8)	O2ⁱ—Cs1—O2^lxxii	58.9 (8)
O1^vi—Cs1—O2^xxxix	60.3 (9)	O2^xxix—Cs1—O2^xxx	91.9 (7)
O1^vi—Cs1—O2^xl	35.0 (9)	O2^xxix—Cs1—O2^xxxii	106.9 (9)
O1^vi—Cs1—O2^xli	89.8 (6)	O2^xxix—Cs1—O2^xxxiv	87.5 (8)
O1^vi—Cs1—O2^xlii	170.5 (9)	O2^xxix—Cs1—O2^xxxv	67.4 (7)
O1^vi—Cs1—O2^xliii	80.5 (7)	O2^xxix—Cs1—O2^xxxvi	118.2 (9)
O1^vi—Cs1—O2^xliv	145.6 (10)	O2^xxix—Cs1—O2^xxxvii	92.5 (8)
O1^vi—Cs1—O2^xlvi	90.2 (6)	O2^xxix—Cs1—O2^xxxviii	154.1 (7)
O1^vi—Cs1—O2^xlvii	34.4 (10)	O2^xxix—Cs1—O2^xxxix	61.8 (9)
O1^vi—Cs1—O2^xlviii	99.5 (7)	O2^xxix—Cs1—O2^xl	112.6 (7)
O1^vi—Cs1—O2^xlix	52.5 (10)	O2^xxix—Cs1—O2^xli	118.2 (9)
O1^vi—Cs1—O2^l	112.5 (6)	O2^xxix—Cs1—O2^xlii	87.5 (8)
O1^vi—Cs1—O2^li	83.4 (7)	O2^xxix—Cs1—O2^xliii	154.1 (7)
O1^vi—Cs1—O2^lii	151.2 (9)	O2^xxix—Cs1—O2^xliv	112.6 (7)
O1^vi—Cs1—O2^liii	67.5 (6)	O2^xxix—Cs1—O2^xlv	92.5 (8)
O1^vi—Cs1—O2^liv	127.5 (10)	O2^xxix—Cs1—O2^xlvi	61.8 (9)
O1^vi—Cs1—O2^lv	28.8 (9)	O2^xxix—Cs1—O2^xlvii	67.4 (7)
O1^vi—Cs1—O2^lvi	96.6 (7)	O2^xxix—Cs1—O2^xlviii	25.9 (7)
O1^vi—Cs1—O2^lvii	109.0 (8)	O2^xxix—Cs1—O2^xlix	69.2 (7)
O1^vi—Cs1—O2^lviii	90.1 (9)	O2^xxix—Cs1—O2^l	29.5 (6)
O1^vi—Cs1—O2^lix	145.0 (9)	O2^xxix—Cs1—O2^li	99.2 (9)
O1^vi—Cs1—O2^lx	119.7 (9)	O2^xxix—Cs1—O2^lii	69.2 (7)
O1^vi—Cs1—O2^lxi	89.9 (9)	O2^xxix—Cs1—O2^liii	150.5 (6)
O1^vi—Cs1—O2^lxii	71.0 (8)	O2^xxix—Cs1—O2^liv	110.8 (7)
O1^vi—Cs1—O2^lxiii	60.3 (9)	O2^xxix—Cs1—O2^lv	110.8 (7)
O1^vi—Cs1—O2^lxv	80.5 (7)	O2^xxix—Cs1—O2^lvi	80.8 (9)
O1^vi—Cs1—O2^lxvi	145.6 (10)	O2^xxix—Cs1—O2^lvii	97.4 (9)
O1^vi—Cs1—O2^lxvii	89.8 (6)	O2^xxix—Cs1—O2^lviii	170.0 (9)
O1^vi—Cs1—O2^lxviii	170.5 (9)	O2^xxix—Cs1—O2^lix	82.6 (9)
O1^vi—Cs1—O2^lxix	34.4 (10)	O2^xxix—Cs1—O2^lx	136.7 (8)
O1^vi—Cs1—O2^lxx	99.5 (7)	O2^xxix—Cs1—O2^lxii	82.6 (9)
O1^vi—Cs1—O2^lxxii	90.2 (6)	O2^xxix—Cs1—O2^lxiii	43.3 (8)
O1^vii—Cs1—O1^viii	154.0 (11)	O2^xxix—Cs1—O2^lxiv	97.4 (9)
O1^vii—Cs1—O1^ix	87.1 (3)	O2^xxix—Cs1—O2^lxv	58.9 (8)
O1^vii—Cs1—O1^x	118.3 (9)	O2^xxix—Cs1—O2^lxvi	121.1 (8)
O1^vii—Cs1—O1^xi	99.5 (9)	O2^xxix—Cs1—O2^lxvii	19.3 (9)
O1^vii—Cs1—O1^xii	61.7 (9)	O2^xxix—Cs1—O2^lxviii	95.1 (6)
O1^vii—Cs1—O1^xiii	38.3 (10)	O2^xxix—Cs1—O2^lxix	58.9 (8)
O1^vii—Cs1—O1^xiv	141.7 (10)	O2^xxix—Cs1—O2^lxx	121.1 (8)
O1^vii—Cs1—O1^xv	118.3 (9)	O2^xxix—Cs1—O2^lxxi	84.9 (6)
O1^vii—Cs1—O1^xvi	80.5 (9)	O2^xxix—Cs1—O2^lxxii	160.7 (9)
O1^vii—Cs1—O1^xvii	61.7 (9)	O2^xxx—Cs1—O2^xxxi	106.9 (9)
O1^vii—Cs1—O1^xviii	80.5 (9)	O2^xxx—Cs1—O2^xxxii	42.0 (7)
O1^vii—Cs1—O1^xix	61.7 (9)	O2^xxx—Cs1—O2^xxxiii	67.4 (7)
O1^vii—Cs1—O1^xx	141.7 (10)	O2^xxx—Cs1—O2^xxxiv	118.2 (9)
O1^vii—Cs1—O1^xxi	118.3 (9)	O2^xxx—Cs1—O2^xxxv	25.9 (7)
O1^vii—Cs1—O1^xxii	61.7 (9)	O2^xxx—Cs1—O2^xxxvi	87.5 (8)
O1^vii—Cs1—O1^xxiii	38.3 (10)	O2^xxx—Cs1—O2^xxxvii	61.8 (9)
O1^vii—Cs1—O1^xxiv	118.3 (9)	O2^xxx—Cs1—O2^xxxviii	112.6 (7)
O1^vii—Cs1—O1^xxv	99.5 (9)	O2^xxx—Cs1—O2^xxxix	92.5 (8)
O1^vii—Cs1—O2^xxvi	96.6 (7)	O2^xxx—Cs1—O2^xl	154.1 (7)
O1^vii—Cs1—O2^xxvii	28.8 (9)	O2^xxx—Cs1—O2^xli	67.4 (7)
O1^vii—Cs1—O2^xxviii	127.5 (10)	O2^xxx—Cs1—O2^xlii	25.9 (7)
O1^vii—Cs1—O2ⁱ	67.5 (6)	O2^xxx—Cs1—O2^xliii	92.5 (8)
O1^vii—Cs1—O2^xxix	151.2 (9)	O2^xxx—Cs1—O2^xliv	61.8 (9)
O1^vii—Cs1—O2^xxx	83.4 (7)	O2^xxx—Cs1—O2^xlv	154.1 (7)
O1^vii—Cs1—O2^xxxi	112.5 (6)	O2^xxx—Cs1—O2^xlvi	112.6 (7)
O1^vii—Cs1—O2^xxxii	52.5 (10)	O2^xxx—Cs1—O2^xlvii	118.2 (9)
O1^vii—Cs1—O2^xxxiii	145.0 (9)	O2^xxx—Cs1—O2^xlviii	87.5 (8)
O1^vii—Cs1—O2^xxxiv	119.7 (9)	O2^xxx—Cs1—O2^xlix	99.2 (9)
O1^vii—Cs1—O2^xxxv	109.0 (8)	O2^xxx—Cs1—O2^l	69.2 (7)
O1^vii—Cs1—O2^xxxvi	90.1 (9)	O2^xxx—Cs1—O2^li	69.2 (7)
O1^vii—Cs1—O2^xxxvii	60.3 (9)	O2^xxx—Cs1—O2^lii	29.5 (6)
O1^vii—Cs1—O2^xxxviii	35.0 (9)	O2^xxx—Cs1—O2^liii	110.8 (7)
O1^vii—Cs1—O2^xxxix	89.9 (9)	O2^xxx—Cs1—O2^liv	80.8 (9)
O1^vii—Cs1—O2^xl	71.0 (8)	O2^xxx—Cs1—O2^lv	150.5 (6)
O1^vii—Cs1—O2^xli	34.4 (10)	O2^xxx—Cs1—O2^lvi	110.8 (7)
O1^vii—Cs1—O2^xlii	99.5 (7)	O2^xxx—Cs1—O2^lviii	97.4 (9)
O1^vii—Cs1—O2^xliii	9.5 (9)	O2^xxx—Cs1—O2^lix	10.0 (9)
O1^vii—Cs1—O2^xliv	90.2 (6)	O2^xxx—Cs1—O2^lx	82.6 (9)
O1^vii—Cs1—O2^xlv	80.5 (7)	O2^xxx—Cs1—O2^lxi	82.6 (9)
O1^vii—Cs1—O2^xlvi	145.6 (10)	O2^xxx—Cs1—O2^lxii	136.7 (8)
O1^vii—Cs1—O2^xlvii	89.8 (6)	O2^xxx—Cs1—O2^lxiii	97.4 (9)
O1^vii—Cs1—O2^xlviii	170.5 (9)	O2^xxx—Cs1—O2^lxiv	170.0 (9)
O1^vii—Cs1—O2^xlix	83.4 (7)	O2^xxx—Cs1—O2^lxv	121.1 (8)
O1^vii—Cs1—O2^l	151.2 (9)	O2^xxx—Cs1—O2^lxvi	58.9 (8)
O1^vii—Cs1—O2^li	52.5 (10)	O2^xxx—Cs1—O2^lxvii	95.1 (6)
O1^vii—Cs1—O2^lii	112.5 (6)	O2^xxx—Cs1—O2^lxviii	19.3 (9)
O1^vii—Cs1—O2^liii	28.8 (9)	O2^xxx—Cs1—O2^lxix	121.1 (8)
O1^vii—Cs1—O2^liv	96.6 (7)	O2^xxx—Cs1—O2^lxx	58.9 (8)
O1^vii—Cs1—O2^lv	67.5 (6)	O2^xxx—Cs1—O2^lxxi	160.7 (9)
O1^vii—Cs1—O2^lvi	127.5 (10)	O2^xxx—Cs1—O2^lxxii	84.9 (6)
O1^vii—Cs1—O2^lvii	60.3 (9)	O2^xxxi—Cs1—O2^xxxii	91.9 (7)
O1^vii—Cs1—O2^lviii	35.0 (9)	O2^xxxi—Cs1—O2^xxxiii	61.8 (9)
O1^vii—Cs1—O2^lix	89.9 (9)	O2^xxxi—Cs1—O2^xxxiv	112.6 (7)
O1^vii—Cs1—O2^lx	71.0 (8)	O2^xxxi—Cs1—O2^xxxv	92.5 (8)
O1^vii—Cs1—O2^lxi	145.0 (9)	O2^xxxi—Cs1—O2^xxxvi	154.1 (7)
O1^vii—Cs1—O2^lxii	119.7 (9)	O2^xxxi—Cs1—O2^xxxvii	67.4 (7)
O1^vii—Cs1—O2^lxiii	109.0 (8)	O2^xxxi—Cs1—O2^xxxviii	118.2 (9)
O1^vii—Cs1—O2^lxiv	90.1 (9)	O2^xxxi—Cs1—O2^xxxix	25.9 (7)
O1^vii—Cs1—O2^lxv	145.6 (10)	O2^xxxi—Cs1—O2^xl	87.5 (8)
O1^vii—Cs1—O2^lxvi	80.5 (7)	O2^xxxi—Cs1—O2^xli	87.5 (8)
O1^vii—Cs1—O2^lxvii	170.5 (9)	O2^xxxi—Cs1—O2^xlii	118.2 (9)
O1^vii—Cs1—O2^lxviii	89.8 (6)	O2^xxxi—Cs1—O2^xliii	112.6 (7)
O1^vii—Cs1—O2^lxix	99.5 (7)	O2^xxxi—Cs1—O2^xliv	154.1 (7)
O1^vii—Cs1—O2^lxx	34.4 (10)	O2^xxxi—Cs1—O2^xlv	61.8 (9)
O1^vii—Cs1—O2^lxxi	90.2 (6)	O2^xxxi—Cs1—O2^xlvi	92.5 (8)
O1^viii—Cs1—O1^ix	87.1 (3)	O2^xxxi—Cs1—O2^xlviii	67.4 (7)
O1^viii—Cs1—O1^x	80.5 (9)	O2^xxxi—Cs1—O2^l	69.2 (7)
O1^viii—Cs1—O1^xi	61.7 (9)	O2^xxxi—Cs1—O2^li	69.2 (7)
O1^viii—Cs1—O1^xii	141.7 (10)	O2^xxxi—Cs1—O2^lii	99.2 (9)
O1^viii—Cs1—O1^xiii	118.3 (9)	O2^xxxi—Cs1—O2^liii	110.8 (7)
O1^viii—Cs1—O1^xiv	61.7 (9)	O2^xxxi—Cs1—O2^liv	150.5 (6)
O1^viii—Cs1—O1^xv	38.3 (10)	O2^xxxi—Cs1—O2^lv	80.8 (9)
O1^viii—Cs1—O1^xvi	118.3 (9)	O2^xxxi—Cs1—O2^lvi	110.8 (7)
O1^viii—Cs1—O1^xvii	99.5 (9)	O2^xxxi—Cs1—O2^lvii	82.6 (9)
O1^viii—Cs1—O1^xviii	118.3 (9)	O2^xxxi—Cs1—O2^lviii	136.7 (8)
O1^viii—Cs1—O1^xix	99.5 (9)	O2^xxxi—Cs1—O2^lix	97.4 (9)
O1^viii—Cs1—O1^xx	61.7 (9)	O2^xxxi—Cs1—O2^lx	170.0 (9)
O1^viii—Cs1—O1^xxi	38.3 (10)	O2^xxxi—Cs1—O2^lxi	43.3 (8)
O1^viii—Cs1—O1^xxii	141.7 (10)	O2^xxxi—Cs1—O2^lxii	97.4 (9)
O1^viii—Cs1—O1^xxiii	118.3 (9)	O2^xxxi—Cs1—O2^lxiii	10.0 (9)
O1^viii—Cs1—O1^xxiv	80.5 (9)	O2^xxxi—Cs1—O2^lxiv	82.6 (9)
O1^viii—Cs1—O1^xxv	61.7 (9)	O2^xxxi—Cs1—O2^lxv	84.9 (6)
O1^viii—Cs1—O2^xxvi	67.5 (6)	O2^xxxi—Cs1—O2^lxvi	160.7 (9)
O1^viii—Cs1—O2^xxvii	127.5 (10)	O2^xxxi—Cs1—O2^lxvii	58.9 (8)
O1^viii—Cs1—O2^xxviii	28.8 (9)	O2^xxxi—Cs1—O2^lxviii	121.1 (8)
O1^viii—Cs1—O2ⁱ	96.6 (7)	O2^xxxi—Cs1—O2^lxix	19.3 (9)
O1^viii—Cs1—O2^xxix	52.5 (10)	O2^xxxi—Cs1—O2^lxx	95.1 (6)
O1^viii—Cs1—O2^xxx	112.5 (6)	O2^xxxi—Cs1—O2^lxxi	58.9 (8)
O1^viii—Cs1—O2^xxxi	83.4 (7)	O2^xxxi—Cs1—O2^lxxii	121.1 (8)
O1^viii—Cs1—O2^xxxii	151.2 (9)	O2^xxxii—Cs1—O2^xxxiii	92.5 (8)
O1^viii—Cs1—O2^xxxiii	60.3 (9)	O2^xxxii—Cs1—O2^xxxiv	154.1 (7)
O1^viii—Cs1—O2^xxxiv	35.0 (9)	O2^xxxii—Cs1—O2^xxxv	61.8 (9)
O1^viii—Cs1—O2^xxxv	89.9 (9)	O2^xxxii—Cs1—O2^xxxvi	112.6 (7)
O1^viii—Cs1—O2^xxxvi	71.0 (8)	O2^xxxii—Cs1—O2^xxxvii	25.9 (7)
O1^viii—Cs1—O2^xxxvii	145.0 (9)	O2^xxxii—Cs1—O2^xxxviii	87.5 (8)
O1^viii—Cs1—O2^xxxviii	119.7 (9)	O2^xxxii—Cs1—O2^xxxix	67.4 (7)
O1^viii—Cs1—O2^xxxix	109.0 (8)	O2^xxxii—Cs1—O2^xl	118.2 (9)
O1^viii—Cs1—O2^xl	90.1 (9)	O2^xxxii—Cs1—O2^xli	25.9 (7)
O1^viii—Cs1—O2^xli	170.5 (9)	O2^xxxii—Cs1—O2^xlii	67.4 (7)
O1^viii—Cs1—O2^xlii	89.8 (6)	O2^xxxii—Cs1—O2^xliii	61.8 (9)
O1^viii—Cs1—O2^xliii	145.6 (10)	O2^xxxii—Cs1—O2^xliv	92.5 (8)
O1^viii—Cs1—O2^xliv	80.5 (7)	O2^xxxii—Cs1—O2^xlv	112.6 (7)
O1^viii—Cs1—O2^xlv	90.2 (6)	O2^xxxii—Cs1—O2^xlvi	154.1 (7)
O1^viii—Cs1—O2^xlvi	9.5 (9)	O2^xxxii—Cs1—O2^xlvii	87.5 (8)
O1^viii—Cs1—O2^xlvii	99.5 (7)	O2^xxxii—Cs1—O2^xlviii	118.2 (9)
O1^viii—Cs1—O2^xlviii	34.4 (10)	O2^xxxii—Cs1—O2^xlix	69.2 (7)
O1^viii—Cs1—O2^xlix	112.5 (6)	O2^xxxii—Cs1—O2^l	99.2 (9)
O1^viii—Cs1—O2^l	52.5 (10)	O2^xxxii—Cs1—O2^li	29.5 (6)
O1^viii—Cs1—O2^li	151.2 (9)	O2^xxxii—Cs1—O2^lii	69.2 (7)
O1^viii—Cs1—O2^lii	83.4 (7)	O2^xxxii—Cs1—O2^liii	80.8 (9)
O1^viii—Cs1—O2^liii	127.5 (10)	O2^xxxii—Cs1—O2^liv	110.8 (7)
O1^viii—Cs1—O2^liv	67.5 (6)	O2^xxxii—Cs1—O2^lv	110.8 (7)
O1^viii—Cs1—O2^lv	96.6 (7)	O2^xxxii—Cs1—O2^lvi	150.5 (6)
O1^viii—Cs1—O2^lvi	28.8 (9)	O2^xxxii—Cs1—O2^lvii	10.0 (9)
O1^viii—Cs1—O2^lvii	145.0 (9)	O2^xxxii—Cs1—O2^lviii	82.6 (9)
O1^viii—Cs1—O2^lviii	119.7 (9)	O2^xxxii—Cs1—O2^lix	43.3 (8)
O1^viii—Cs1—O2^lix	109.0 (8)	O2^xxxii—Cs1—O2^lx	97.4 (9)
O1^viii—Cs1—O2^lx	90.1 (9)	O2^xxxii—Cs1—O2^lxi	97.4 (9)
O1^viii—Cs1—O2^lxi	60.3 (9)	O2^xxxii—Cs1—O2^lxii	170.0 (9)
O1^viii—Cs1—O2^lxiii	89.9 (9)	O2^xxxii—Cs1—O2^lxiii	82.6 (9)
O1^viii—Cs1—O2^lxiv	71.0 (8)	O2^xxxii—Cs1—O2^lxiv	136.7 (8)
O1^viii—Cs1—O2^lxvi	90.2 (6)	O2^xxxii—Cs1—O2^lxv	160.7 (9)
O1^viii—Cs1—O2^lxviii	99.5 (7)	O2^xxxii—Cs1—O2^lxvi	84.9 (6)
O1^viii—Cs1—O2^lxix	89.8 (6)	O2^xxxii—Cs1—O2^lxvii	121.1 (8)
O1^viii—Cs1—O2^lxx	170.5 (9)	O2^xxxii—Cs1—O2^lxviii	58.9 (8)
O1^viii—Cs1—O2^lxxi	80.5 (7)	O2^xxxii—Cs1—O2^lxix	95.1 (6)
O1^viii—Cs1—O2^lxxii	145.6 (10)	O2^xxxii—Cs1—O2^lxx	19.3 (9)
O1^ix—Cs1—O1^x	141.7 (10)	O2^xxxii—Cs1—O2^lxxi	121.1 (8)
O1^ix—Cs1—O1^xi	118.3 (9)	O2^xxxiii—Cs1—O2^xxxiv	91.9 (7)
O1^ix—Cs1—O1^xii	80.5 (9)	O2^xxxiii—Cs1—O2^xxxv	42.0 (7)
O1^ix—Cs1—O1^xiii	61.7 (9)	O2^xxxiii—Cs1—O2^xxxvi	106.9 (9)
O1^ix—Cs1—O1^xiv	118.3 (9)	O2^xxxiii—Cs1—O2^xxxvii	88.1 (7)
O1^ix—Cs1—O1^xv	99.5 (9)	O2^xxxiii—Cs1—O2^xxxviii	180
O1^ix—Cs1—O1^xvi	61.7 (9)	O2^xxxiii—Cs1—O2^xxxix	73.1 (9)
O1^ix—Cs1—O1^xvii	38.3 (10)	O2^xxxiii—Cs1—O2^xl	138.0 (7)
O1^ix—Cs1—O1^xviii	141.7 (10)	O2^xxxiii—Cs1—O2^xli	112.6 (7)
O1^ix—Cs1—O1^xix	118.3 (9)	O2^xxxiii—Cs1—O2^xlii	61.8 (9)
O1^ix—Cs1—O1^xx	80.5 (9)	O2^xxxiii—Cs1—O2^xliii	154.1 (7)
O1^ix—Cs1—O1^xxi	61.7 (9)	O2^xxxiii—Cs1—O2^xliv	92.5 (8)
O1^ix—Cs1—O1^xxii	118.3 (9)	O2^xxxiii—Cs1—O2^xlv	118.2 (9)
O1^ix—Cs1—O1^xxiii	99.5 (9)	O2^xxxiii—Cs1—O2^xlvi	67.4 (7)
O1^ix—Cs1—O1^xxiv	61.7 (9)	O2^xxxiii—Cs1—O2^xlvii	87.5 (8)
O1^ix—Cs1—O2^xxvi	127.5 (10)	O2^xxxiii—Cs1—O2^xlviii	25.9 (7)
O1^ix—Cs1—O2^xxvii	67.5 (6)	O2^xxxiii—Cs1—O2^xlix	82.6 (9)
O1^ix—Cs1—O2^xxviii	96.6 (7)	O2^xxxiii—Cs1—O2^l	10.0 (9)
O1^ix—Cs1—O2^xxix	112.5 (6)	O2^xxxiii—Cs1—O2^li	97.4 (9)
O1^ix—Cs1—O2^xxx	52.5 (10)	O2^xxxiii—Cs1—O2^liii	170.0 (9)
O1^ix—Cs1—O2^xxxi	151.2 (9)	O2^xxxiii—Cs1—O2^liv	97.4 (9)
O1^ix—Cs1—O2^xxxii	83.4 (7)	O2^xxxiii—Cs1—O2^lv	136.7 (8)
O1^ix—Cs1—O2^xxxiii	89.9 (9)	O2^xxxiii—Cs1—O2^lvi	82.6 (9)
O1^ix—Cs1—O2^xxxiv	71.0 (8)	O2^xxxiii—Cs1—O2^lvii	84.9 (6)
O1^ix—Cs1—O2^xxxv	60.3 (9)	O2^xxxiii—Cs1—O2^lviii	160.7 (9)
O1^ix—Cs1—O2^xxxvi	35.0 (9)	O2^xxxiii—Cs1—O2^lix	58.9 (8)
O1^ix—Cs1—O2^xxxvii	109.0 (8)	O2^xxxiii—Cs1—O2^lx	121.1 (8)
O1^ix—Cs1—O2^xxxviii	90.1 (9)	O2^xxxiii—Cs1—O2^lxii	95.1 (6)
O1^ix—Cs1—O2^xxxix	145.0 (9)	O2^xxxiii—Cs1—O2^lxiii	58.9 (8)
O1^ix—Cs1—O2^xl	119.7 (9)	O2^xxxiii—Cs1—O2^lxiv	121.1 (8)
O1^ix—Cs1—O2^xli	99.5 (7)	O2^xxxiii—Cs1—O2^lxv	69.2 (7)
O1^ix—Cs1—O2^xlii	34.4 (10)	O2^xxxiii—Cs1—O2^lxvi	99.2 (9)
O1^ix—Cs1—O2^xliii	90.2 (6)	O2^xxxiii—Cs1—O2^lxviii	69.2 (7)
O1^ix—Cs1—O2^xliv	9.5 (9)	O2^xxxiii—Cs1—O2^lxix	80.8 (9)
O1^ix—Cs1—O2^xlv	145.6 (10)	O2^xxxiii—Cs1—O2^lxx	110.8 (7)
O1^ix—Cs1—O2^xlvi	80.5 (7)	O2^xxxiii—Cs1—O2^lxxi	110.8 (7)
O1^ix—Cs1—O2^xlvii	170.5 (9)	O2^xxxiii—Cs1—O2^lxxii	150.5 (6)
O1^ix—Cs1—O2^xlviii	89.8 (6)	O2^xxxiv—Cs1—O2^xxxv	106.9 (9)
O1^ix—Cs1—O2^xlix	151.2 (9)	O2^xxxiv—Cs1—O2^xxxvii	180
O1^ix—Cs1—O2^l	83.4 (7)	O2^xxxiv—Cs1—O2^xxxviii	88.1 (7)
O1^ix—Cs1—O2^li	112.5 (6)	O2^xxxiv—Cs1—O2^xxxix	138.0 (7)
O1^ix—Cs1—O2^lii	52.5 (10)	O2^xxxiv—Cs1—O2^xl	73.1 (9)
O1^ix—Cs1—O2^liii	96.6 (7)	O2^xxxiv—Cs1—O2^xli	154.1 (7)
O1^ix—Cs1—O2^liv	28.8 (9)	O2^xxxiv—Cs1—O2^xlii	92.5 (8)
O1^ix—Cs1—O2^lv	127.5 (10)	O2^xxxiv—Cs1—O2^xliii	112.6 (7)
O1^ix—Cs1—O2^lvi	67.5 (6)	O2^xxxiv—Cs1—O2^xliv	61.8 (9)
O1^ix—Cs1—O2^lvii	89.9 (9)	O2^xxxiv—Cs1—O2^xlv	87.5 (8)
O1^ix—Cs1—O2^lviii	71.0 (8)	O2^xxxiv—Cs1—O2^xlvii	118.2 (9)
O1^ix—Cs1—O2^lix	60.3 (9)	O2^xxxiv—Cs1—O2^xlviii	67.4 (7)
O1^ix—Cs1—O2^lx	35.0 (9)	O2^xxxiv—Cs1—O2^xlix	136.7 (8)
O1^ix—Cs1—O2^lxi	109.0 (8)	O2^xxxiv—Cs1—O2^l	82.6 (9)
O1^ix—Cs1—O2^lxii	90.1 (9)	O2^xxxiv—Cs1—O2^li	170.0 (9)
O1^ix—Cs1—O2^lxiii	145.0 (9)	O2^xxxiv—Cs1—O2^lii	97.4 (9)
O1^ix—Cs1—O2^lxiv	119.7 (9)	O2^xxxiv—Cs1—O2^liii	97.4 (9)
O1^ix—Cs1—O2^lxv	90.2 (6)	O2^xxxiv—Cs1—O2^liv	43.3 (8)
O1^ix—Cs1—O2^lxvi	9.5 (9)	O2^xxxiv—Cs1—O2^lv	82.6 (9)
O1^ix—Cs1—O2^lxvii	99.5 (7)	O2^xxxiv—Cs1—O2^lvi	10.0 (9)
O1^ix—Cs1—O2^lxviii	34.4 (10)	O2^xxxiv—Cs1—O2^lvii	160.7 (9)
O1^ix—Cs1—O2^lxix	170.5 (9)	O2^xxxiv—Cs1—O2^lviii	84.9 (6)
O1^ix—Cs1—O2^lxx	89.8 (6)	O2^xxxiv—Cs1—O2^lix	121.1 (8)
O1^ix—Cs1—O2^lxxi	145.6 (10)	O2^xxxiv—Cs1—O2^lx	58.9 (8)
O1^ix—Cs1—O2^lxxii	80.5 (7)	O2^xxxiv—Cs1—O2^lxi	95.1 (6)
O1^x—Cs1—O1^xi	87.1 (3)	O2^xxxiv—Cs1—O2^lxii	19.3 (9)
O1^x—Cs1—O1^xii	87.1 (3)	O2^xxxiv—Cs1—O2^lxiii	121.1 (8)
O1^x—Cs1—O1^xiii	154.0 (11)	O2^xxxiv—Cs1—O2^lxiv	58.9 (8)
O1^x—Cs1—O1^xv	92.9 (3)	O2^xxxiv—Cs1—O2^lxvi	69.2 (7)
O1^x—Cs1—O1^xvi	92.9 (3)	O2^xxxiv—Cs1—O2^lxvii	69.2 (7)
O1^x—Cs1—O1^xvii	180	O2^xxxiv—Cs1—O2^lxviii	99.2 (9)
O1^x—Cs1—O1^xix	99.5 (9)	O2^xxxiv—Cs1—O2^lxix	110.8 (7)
O1^x—Cs1—O1^xx	61.7 (9)	O2^xxxiv—Cs1—O2^lxx	150.5 (6)
O1^x—Cs1—O1^xxi	118.3 (9)	O2^xxxiv—Cs1—O2^lxxi	80.8 (9)
O1^x—Cs1—O1^xxii	61.7 (9)	O2^xxxiv—Cs1—O2^lxxii	110.8 (7)
O1^x—Cs1—O1^xxiii	118.3 (9)	O2^xxxv—Cs1—O2^xxxvi	91.9 (7)
O1^x—Cs1—O1^xxiv	80.5 (9)	O2^xxxv—Cs1—O2^xxxvii	73.1 (9)
O1^x—Cs1—O1^xxv	141.7 (10)	O2^xxxv—Cs1—O2^xxxviii	138.0 (7)
O1^x—Cs1—O2^xxvi	80.5 (7)	O2^xxxv—Cs1—O2^xxxix	88.1 (7)
O1^x—Cs1—O2^xxvii	145.6 (10)	O2^xxxv—Cs1—O2^xl	180
O1^x—Cs1—O2^xxviii	89.8 (6)	O2^xxxv—Cs1—O2^xli	87.5 (8)
O1^x—Cs1—O2ⁱ	170.5 (9)	O2^xxxv—Cs1—O2^xliii	118.2 (9)
O1^x—Cs1—O2^xxx	99.5 (7)	O2^xxxv—Cs1—O2^xliv	67.4 (7)
O1^x—Cs1—O2^xxxii	90.2 (6)	O2^xxxv—Cs1—O2^xlv	154.1 (7)
O1^x—Cs1—O2^xxxiii	52.5 (10)	O2^xxxv—Cs1—O2^xlvi	92.5 (8)
O1^x—Cs1—O2^xxxiv	112.5 (6)	O2^xxxv—Cs1—O2^xlvii	112.6 (7)
O1^x—Cs1—O2^xxxv	83.4 (7)	O2^xxxv—Cs1—O2^xlviii	61.8 (9)
O1^x—Cs1—O2^xxxvi	151.2 (9)	O2^xxxv—Cs1—O2^xlix	97.4 (9)
O1^x—Cs1—O2^xxxvii	67.5 (6)	O2^xxxv—Cs1—O2^l	43.3 (8)
O1^x—Cs1—O2^xxxviii	127.5 (10)	O2^xxxv—Cs1—O2^li	82.6 (9)
O1^x—Cs1—O2^xxxix	28.8 (9)	O2^xxxv—Cs1—O2^lii	10.0 (9)
O1^x—Cs1—O2^xl	96.6 (7)	O2^xxxv—Cs1—O2^liii	136.7 (8)
O1^x—Cs1—O2^xli	90.1 (9)	O2^xxxv—Cs1—O2^liv	82.6 (9)
O1^x—Cs1—O2^xlii	109.0 (8)	O2^xxxv—Cs1—O2^lv	170.0 (9)
O1^x—Cs1—O2^xliii	119.7 (9)	O2^xxxv—Cs1—O2^lvi	97.4 (9)
O1^x—Cs1—O2^xliv	145.0 (9)	O2^xxxv—Cs1—O2^lvii	58.9 (8)
O1^x—Cs1—O2^xlv	71.0 (8)	O2^xxxv—Cs1—O2^lviii	121.1 (8)
O1^x—Cs1—O2^xlvi	89.9 (9)	O2^xxxv—Cs1—O2^lix	19.3 (9)
O1^x—Cs1—O2^xlvii	35.0 (9)	O2^xxxv—Cs1—O2^lx	95.1 (6)
O1^x—Cs1—O2^xlviii	60.3 (9)	O2^xxxv—Cs1—O2^lxi	58.9 (8)
O1^x—Cs1—O2^xlix	35.0 (9)	O2^xxxv—Cs1—O2^lxii	121.1 (8)
O1^x—Cs1—O2^l	60.3 (9)	O2^xxxv—Cs1—O2^lxiii	84.9 (6)
O1^x—Cs1—O2^li	71.0 (8)	O2^xxxv—Cs1—O2^lxiv	160.7 (9)
O1^x—Cs1—O2^lii	89.9 (9)	O2^xxxv—Cs1—O2^lxv	99.2 (9)
O1^x—Cs1—O2^liii	119.7 (9)	O2^xxxv—Cs1—O2^lxvi	69.2 (7)
O1^x—Cs1—O2^liv	145.0 (9)	O2^xxxv—Cs1—O2^lxvii	69.2 (7)
O1^x—Cs1—O2^lv	90.1 (9)	O2^xxxv—Cs1—O2^lxviii	29.5 (6)
O1^x—Cs1—O2^lvi	109.0 (8)	O2^xxxv—Cs1—O2^lxix	110.8 (7)
O1^x—Cs1—O2^lvii	80.5 (7)	O2^xxxv—Cs1—O2^lxx	80.8 (9)
O1^x—Cs1—O2^lviii	145.6 (10)	O2^xxxv—Cs1—O2^lxxi	150.5 (6)
O1^x—Cs1—O2^lix	89.8 (6)	O2^xxxv—Cs1—O2^lxxii	110.8 (7)
O1^x—Cs1—O2^lx	170.5 (9)	O2^xxxvi—Cs1—O2^xxxvii	138.0 (7)
O1^x—Cs1—O2^lxii	99.5 (7)	O2^xxxvi—Cs1—O2^xxxviii	73.1 (9)
O1^x—Cs1—O2^lxiv	90.2 (6)	O2^xxxvi—Cs1—O2^xxxix	180
O1^x—Cs1—O2^lxv	83.4 (7)	O2^xxxvi—Cs1—O2^xl	88.1 (7)
O1^x—Cs1—O2^lxvi	151.2 (9)	O2^xxxvi—Cs1—O2^xli	118.2 (9)
O1^x—Cs1—O2^lxvii	52.5 (10)	O2^xxxvi—Cs1—O2^xlii	67.4 (7)
O1^x—Cs1—O2^lxviii	112.5 (6)	O2^xxxvi—Cs1—O2^xliii	87.5 (8)
O1^x—Cs1—O2^lxx	96.6 (7)	O2^xxxvi—Cs1—O2^xliv	25.9 (7)
O1^x—Cs1—O2^lxxi	67.5 (6)	O2^xxxvi—Cs1—O2^xlv	112.6 (7)
O1^x—Cs1—O2^lxxii	127.5 (10)	O2^xxxvi—Cs1—O2^xlvi	61.8 (9)
O1^xi—Cs1—O1^xii	154.0 (11)	O2^xxxvi—Cs1—O2^xlvii	154.1 (7)
O1^xi—Cs1—O1^xiii	87.1 (3)	O2^xxxvi—Cs1—O2^xlviii	92.5 (8)
O1^xi—Cs1—O1^xiv	92.9 (3)	O2^xxxvi—Cs1—O2^xlix	170.0 (9)
O1^xi—Cs1—O1^xv	26.0 (11)	O2^xxxvi—Cs1—O2^l	97.4 (9)
O1^xi—Cs1—O1^xvi	180	O2^xxxvi—Cs1—O2^li	136.7 (8)
O1^xi—Cs1—O1^xvii	92.9 (3)	O2^xxxvi—Cs1—O2^lii	82.6 (9)
O1^xi—Cs1—O1^xviii	99.5 (9)	O2^xxxvi—Cs1—O2^liii	82.6 (9)
O1^xi—Cs1—O1^xix	38.3 (10)	O2^xxxvi—Cs1—O2^liv	10.0 (9)
O1^xi—Cs1—O1^xx	118.3 (9)	O2^xxxvi—Cs1—O2^lv	97.4 (9)
O1^xi—Cs1—O1^xxi	61.7 (9)	O2^xxxvi—Cs1—O2^lvi	43.3 (8)
O1^xi—Cs1—O1^xxii	118.3 (9)	O2^xxxvi—Cs1—O2^lvii	121.1 (8)
O1^xi—Cs1—O1^xxiii	61.7 (9)	O2^xxxvi—Cs1—O2^lviii	58.9 (8)
O1^xi—Cs1—O1^xxiv	141.7 (10)	O2^xxxvi—Cs1—O2^lix	95.1 (6)
O1^xi—Cs1—O1^xxv	80.5 (9)	O2^xxxvi—Cs1—O2^lx	19.3 (9)
O1^xi—Cs1—O2^xxvii	90.2 (6)	O2^xxxvi—Cs1—O2^lxi	121.1 (8)
O1^xi—Cs1—O2ⁱ	99.5 (7)	O2^xxxvi—Cs1—O2^lxii	58.9 (8)
O1^xi—Cs1—O2^xxix	89.8 (6)	O2^xxxvi—Cs1—O2^lxiii	160.7 (9)
O1^xi—Cs1—O2^xxx	170.5 (9)	O2^xxxvi—Cs1—O2^lxiv	84.9 (6)
O1^xi—Cs1—O2^xxxi	80.5 (7)	O2^xxxvi—Cs1—O2^lxv	69.2 (7)
O1^xi—Cs1—O2^xxxii	145.6 (10)	O2^xxxvi—Cs1—O2^lxvi	29.5 (6)
O1^xi—Cs1—O2^xxxiii	112.5 (6)	O2^xxxvi—Cs1—O2^lxvii	99.2 (9)
O1^xi—Cs1—O2^xxxiv	52.5 (10)	O2^xxxvi—Cs1—O2^lxviii	69.2 (7)
O1^xi—Cs1—O2^xxxv	151.2 (9)	O2^xxxvi—Cs1—O2^lxix	150.5 (6)
O1^xi—Cs1—O2^xxxvi	83.4 (7)	O2^xxxvi—Cs1—O2^lxx	110.8 (7)
O1^xi—Cs1—O2^xxxvii	127.5 (10)	O2^xxxvi—Cs1—O2^lxxi	110.8 (7)
O1^xi—Cs1—O2^xxxviii	67.5 (6)	O2^xxxvi—Cs1—O2^lxxii	80.8 (9)
O1^xi—Cs1—O2^xxxix	96.6 (7)	O2^xxxvii—Cs1—O2^xxxviii	91.9 (7)
O1^xi—Cs1—O2^xli	119.7 (9)	O2^xxxvii—Cs1—O2^xxxix	42.0 (7)
O1^xi—Cs1—O2^xlii	145.0 (9)	O2^xxxvii—Cs1—O2^xl	106.9 (9)
O1^xi—Cs1—O2^xliii	90.1 (9)	O2^xxxvii—Cs1—O2^xli	25.9 (7)
O1^xi—Cs1—O2^xliv	109.0 (8)	O2^xxxvii—Cs1—O2^xlii	87.5 (8)
O1^xi—Cs1—O2^xlv	35.0 (9)	O2^xxxvii—Cs1—O2^xliii	67.4 (7)
O1^xi—Cs1—O2^xlvi	60.3 (9)	O2^xxxvii—Cs1—O2^xliv	118.2 (9)
O1^xi—Cs1—O2^xlvii	71.0 (8)	O2^xxxvii—Cs1—O2^xlv	92.5 (8)
O1^xi—Cs1—O2^xlviii	89.9 (9)	O2^xxxvii—Cs1—O2^xlvi	154.1 (7)
O1^xi—Cs1—O2^xlix	90.1 (9)	O2^xxxvii—Cs1—O2^xlvii	61.8 (9)
O1^xi—Cs1—O2^l	109.0 (8)	O2^xxxvii—Cs1—O2^xlviii	112.6 (7)
O1^xi—Cs1—O2^li	119.7 (9)	O2^xxxvii—Cs1—O2^xlix	43.3 (8)
O1^xi—Cs1—O2^lii	145.0 (9)	O2^xxxvii—Cs1—O2^l	97.4 (9)
O1^xi—Cs1—O2^liii	71.0 (8)	O2^xxxvii—Cs1—O2^li	10.0 (9)
O1^xi—Cs1—O2^liv	89.9 (9)	O2^xxxvii—Cs1—O2^lii	82.6 (9)
O1^xi—Cs1—O2^lv	35.0 (9)	O2^xxxvii—Cs1—O2^liii	82.6 (9)
O1^xi—Cs1—O2^lvi	60.3 (9)	O2^xxxvii—Cs1—O2^liv	136.7 (8)
O1^xi—Cs1—O2^lvii	145.6 (10)	O2^xxxvii—Cs1—O2^lv	97.4 (9)
O1^xi—Cs1—O2^lviii	80.5 (7)	O2^xxxvii—Cs1—O2^lvi	170.0 (9)
O1^xi—Cs1—O2^lix	170.5 (9)	O2^xxxvii—Cs1—O2^lvii	19.3 (9)
O1^xi—Cs1—O2^lx	89.8 (6)	O2^xxxvii—Cs1—O2^lviii	95.1 (6)
O1^xi—Cs1—O2^lxi	99.5 (7)	O2^xxxvii—Cs1—O2^lix	58.9 (8)
O1^xi—Cs1—O2^lxii	34.4 (10)	O2^xxxvii—Cs1—O2^lx	121.1 (8)
O1^xi—Cs1—O2^lxiii	90.2 (6)	O2^xxxvii—Cs1—O2^lxi	84.9 (6)
O1^xi—Cs1—O2^lxiv	9.5 (9)	O2^xxxvii—Cs1—O2^lxii	160.7 (9)
O1^xi—Cs1—O2^lxv	52.5 (10)	O2^xxxvii—Cs1—O2^lxiii	58.9 (8)
O1^xi—Cs1—O2^lxvi	112.5 (6)	O2^xxxvii—Cs1—O2^lxiv	121.1 (8)
O1^xi—Cs1—O2^lxvii	83.4 (7)	O2^xxxvii—Cs1—O2^lxv	150.5 (6)
O1^xi—Cs1—O2^lxviii	151.2 (9)	O2^xxxvii—Cs1—O2^lxvi	110.8 (7)
O1^xi—Cs1—O2^lxix	67.5 (6)	O2^xxxvii—Cs1—O2^lxvii	110.8 (7)
O1^xi—Cs1—O2^lxx	127.5 (10)	O2^xxxvii—Cs1—O2^lxviii	80.8 (9)
O1^xi—Cs1—O2^lxxi	28.8 (9)	O2^xxxvii—Cs1—O2^lxix	69.2 (7)
O1^xi—Cs1—O2^lxxii	96.6 (7)	O2^xxxvii—Cs1—O2^lxx	29.5 (6)
O1^xii—Cs1—O1^xiii	87.1 (3)	O2^xxxvii—Cs1—O2^lxxi	99.2 (9)
O1^xii—Cs1—O1^xiv	92.9 (3)	O2^xxxvii—Cs1—O2^lxxii	69.2 (7)
O1^xii—Cs1—O1^xv	180	O2^xxxviii—Cs1—O2^xxxix	106.9 (9)
O1^xii—Cs1—O1^xvii	92.9 (3)	O2^xxxviii—Cs1—O2^xl	42.0 (7)
O1^xii—Cs1—O1^xviii	61.7 (9)	O2^xxxviii—Cs1—O2^xli	67.4 (7)
O1^xii—Cs1—O1^xix	118.3 (9)	O2^xxxviii—Cs1—O2^xlii	118.2 (9)
O1^xii—Cs1—O1^xx	80.5 (9)	O2^xxxviii—Cs1—O2^xliii	25.9 (7)
O1^xii—Cs1—O1^xxi	141.7 (10)	O2^xxxviii—Cs1—O2^xliv	87.5 (8)
O1^xii—Cs1—O1^xxiii	99.5 (9)	O2^xxxviii—Cs1—O2^xlv	61.8 (9)
O1^xii—Cs1—O1^xxiv	61.7 (9)	O2^xxxviii—Cs1—O2^xlvi	112.6 (7)
O1^xii—Cs1—O1^xxv	118.3 (9)	O2^xxxviii—Cs1—O2^xlvii	92.5 (8)
O1^xii—Cs1—O2^xxvi	145.6 (10)	O2^xxxviii—Cs1—O2^xlviii	154.1 (7)
O1^xii—Cs1—O2^xxvii	80.5 (7)	O2^xxxviii—Cs1—O2^xlix	97.4 (9)
O1^xii—Cs1—O2^xxviii	170.5 (9)	O2^xxxviii—Cs1—O2^l	170.0 (9)
O1^xii—Cs1—O2ⁱ	89.8 (6)	O2^xxxviii—Cs1—O2^li	82.6 (9)
O1^xii—Cs1—O2^xxix	99.5 (7)	O2^xxxviii—Cs1—O2^lii	136.7 (8)
O1^xii—Cs1—O2^xxx	34.4 (10)	O2^xxxviii—Cs1—O2^liii	10.0 (9)
O1^xii—Cs1—O2^xxxi	90.2 (6)	O2^xxxviii—Cs1—O2^liv	82.6 (9)
O1^xii—Cs1—O2^xxxii	9.5 (9)	O2^xxxviii—Cs1—O2^lv	43.3 (8)
O1^xii—Cs1—O2^xxxiii	83.4 (7)	O2^xxxviii—Cs1—O2^lvi	97.4 (9)
O1^xii—Cs1—O2^xxxiv	151.2 (9)	O2^xxxviii—Cs1—O2^lvii	95.1 (6)
O1^xii—Cs1—O2^xxxv	52.5 (10)	O2^xxxviii—Cs1—O2^lviii	19.3 (9)
O1^xii—Cs1—O2^xxxvi	112.5 (6)	O2^xxxviii—Cs1—O2^lix	121.1 (8)
O1^xii—Cs1—O2^xxxviii	96.6 (7)	O2^xxxviii—Cs1—O2^lx	58.9 (8)
O1^xii—Cs1—O2^xxxix	67.5 (6)	O2^xxxviii—Cs1—O2^lxi	160.7 (9)
O1^xii—Cs1—O2^xl	127.5 (10)	O2^xxxviii—Cs1—O2^lxii	84.9 (6)
O1^xii—Cs1—O2^xlii	60.3 (9)	O2^xxxviii—Cs1—O2^lxiii	121.1 (8)
O1^xii—Cs1—O2^xliii	71.0 (8)	O2^xxxviii—Cs1—O2^lxiv	58.9 (8)
O1^xii—Cs1—O2^xliv	89.9 (9)	O2^xxxviii—Cs1—O2^lxv	110.8 (7)
O1^xii—Cs1—O2^xlv	119.7 (9)	O2^xxxviii—Cs1—O2^lxvi	80.8 (9)
O1^xii—Cs1—O2^xlvi	145.0 (9)	O2^xxxviii—Cs1—O2^lxvii	150.5 (6)
O1^xii—Cs1—O2^xlvii	90.1 (9)	O2^xxxviii—Cs1—O2^lxviii	110.8 (7)
O1^xii—Cs1—O2^xlviii	109.0 (8)	O2^xxxviii—Cs1—O2^lxix	99.2 (9)
O1^xii—Cs1—O2^xlix	71.0 (8)	O2^xxxviii—Cs1—O2^lxx	69.2 (7)
O1^xii—Cs1—O2^l	89.9 (9)	O2^xxxviii—Cs1—O2^lxxi	69.2 (7)
O1^xii—Cs1—O2^lii	60.3 (9)	O2^xxxviii—Cs1—O2^lxxii	29.5 (6)
O1^xii—Cs1—O2^liii	90.1 (9)	O2^xxxix—Cs1—O2^xl	91.9 (7)
O1^xii—Cs1—O2^liv	109.0 (8)	O2^xxxix—Cs1—O2^xli	61.8 (9)
O1^xii—Cs1—O2^lv	119.7 (9)	O2^xxxix—Cs1—O2^xlii	112.6 (7)
O1^xii—Cs1—O2^lvi	145.0 (9)	O2^xxxix—Cs1—O2^xliii	92.5 (8)
O1^xii—Cs1—O2^lviii	90.2 (6)	O2^xxxix—Cs1—O2^xliv	154.1 (7)
O1^xii—Cs1—O2^lix	34.4 (10)	O2^xxxix—Cs1—O2^xlv	67.4 (7)
O1^xii—Cs1—O2^lx	99.5 (7)	O2^xxxix—Cs1—O2^xlvi	118.2 (9)
O1^xii—Cs1—O2^lxi	89.8 (6)	O2^xxxix—Cs1—O2^xlvii	25.9 (7)
O1^xii—Cs1—O2^lxii	170.5 (9)	O2^xxxix—Cs1—O2^xlviii	87.5 (8)
O1^xii—Cs1—O2^lxiii	80.5 (7)	O2^xxxix—Cs1—O2^xlix	10.0 (9)
O1^xii—Cs1—O2^lxiv	145.6 (10)	O2^xxxix—Cs1—O2^l	82.6 (9)
O1^xii—Cs1—O2^lxv	151.2 (9)	O2^xxxix—Cs1—O2^li	43.3 (8)
O1^xii—Cs1—O2^lxvi	83.4 (7)	O2^xxxix—Cs1—O2^lii	97.4 (9)
O1^xii—Cs1—O2^lxvii	112.5 (6)	O2^xxxix—Cs1—O2^liii	97.4 (9)
O1^xii—Cs1—O2^lxviii	52.5 (10)	O2^xxxix—Cs1—O2^liv	170.0 (9)
O1^xii—Cs1—O2^lxix	96.6 (7)	O2^xxxix—Cs1—O2^lv	82.6 (9)
O1^xii—Cs1—O2^lxxi	127.5 (10)	O2^xxxix—Cs1—O2^lvi	136.7 (8)
O1^xii—Cs1—O2^lxxii	67.5 (6)	O2^xxxix—Cs1—O2^lvii	58.9 (8)
O1^xiii—Cs1—O1^xiv	180	O2^xxxix—Cs1—O2^lviii	121.1 (8)
O1^xiii—Cs1—O1^xv	92.9 (3)	O2^xxxix—Cs1—O2^lix	84.9 (6)
O1^xiii—Cs1—O1^xvi	92.9 (3)	O2^xxxix—Cs1—O2^lx	160.7 (9)
O1^xiii—Cs1—O1^xvii	26.0 (11)	O2^xxxix—Cs1—O2^lxi	58.9 (8)
O1^xiii—Cs1—O1^xviii	118.3 (9)	O2^xxxix—Cs1—O2^lxii	121.1 (8)
O1^xiii—Cs1—O1^xix	61.7 (9)	O2^xxxix—Cs1—O2^lxiii	19.3 (9)
O1^xiii—Cs1—O1^xx	141.7 (10)	O2^xxxix—Cs1—O2^lxiv	95.1 (6)
O1^xiii—Cs1—O1^xxi	80.5 (9)	O2^xxxix—Cs1—O2^lxv	110.8 (7)
O1^xiii—Cs1—O1^xxii	99.5 (9)	O2^xxxix—Cs1—O2^lxvi	150.5 (6)
O1^xiii—Cs1—O1^xxiii	38.3 (10)	O2^xxxix—Cs1—O2^lxvii	80.8 (9)
O1^xiii—Cs1—O1^xxiv	118.3 (9)	O2^xxxix—Cs1—O2^lxviii	110.8 (7)
O1^xiii—Cs1—O1^xxv	61.7 (9)	O2^xxxix—Cs1—O2^lxix	29.5 (6)
O1^xiii—Cs1—O2^xxvi	90.2 (6)	O2^xxxix—Cs1—O2^lxx	69.2 (7)
O1^xiii—Cs1—O2^xxviii	99.5 (7)	O2^xxxix—Cs1—O2^lxxi	69.2 (7)
O1^xiii—Cs1—O2^xxix	170.5 (9)	O2^xxxix—Cs1—O2^lxxii	99.2 (9)
O1^xiii—Cs1—O2^xxx	89.8 (6)	O2^xl—Cs1—O2^xli	92.5 (8)
O1^xiii—Cs1—O2^xxxi	145.6 (10)	O2^xl—Cs1—O2^xlii	154.1 (7)
O1^xiii—Cs1—O2^xxxii	80.5 (7)	O2^xl—Cs1—O2^xliii	61.8 (9)
O1^xiii—Cs1—O2^xxxiii	151.2 (9)	O2^xl—Cs1—O2^xliv	112.6 (7)
O1^xiii—Cs1—O2^xxxiv	83.4 (7)	O2^xl—Cs1—O2^xlv	25.9 (7)
O1^xiii—Cs1—O2^xxxv	112.5 (6)	O2^xl—Cs1—O2^xlvi	87.5 (8)
O1^xiii—Cs1—O2^xxxvi	52.5 (10)	O2^xl—Cs1—O2^xlvii	67.4 (7)
O1^xiii—Cs1—O2^xxxvii	96.6 (7)	O2^xl—Cs1—O2^xlviii	118.2 (9)
O1^xiii—Cs1—O2^xxxix	127.5 (10)	O2^xl—Cs1—O2^xlix	82.6 (9)
O1^xiii—Cs1—O2^xl	67.5 (6)	O2^xl—Cs1—O2^l	136.7 (8)
O1^xiii—Cs1—O2^xli	71.0 (8)	O2^xl—Cs1—O2^li	97.4 (9)
O1^xiii—Cs1—O2^xlii	89.9 (9)	O2^xl—Cs1—O2^lii	170.0 (9)
O1^xiii—Cs1—O2^xliii	35.0 (9)	O2^xl—Cs1—O2^liii	43.3 (8)
O1^xiii—Cs1—O2^xliv	60.3 (9)	O2^xl—Cs1—O2^liv	97.4 (9)
O1^xiii—Cs1—O2^xlv	90.1 (9)	O2^xl—Cs1—O2^lv	10.0 (9)
O1^xiii—Cs1—O2^xlvi	109.0 (8)	O2^xl—Cs1—O2^lvi	82.6 (9)
O1^xiii—Cs1—O2^xlvii	119.7 (9)	O2^xl—Cs1—O2^lvii	121.1 (8)
O1^xiii—Cs1—O2^xlviii	145.0 (9)	O2^xl—Cs1—O2^lviii	58.9 (8)
O1^xiii—Cs1—O2^xlix	119.7 (9)	O2^xl—Cs1—O2^lix	160.7 (9)
O1^xiii—Cs1—O2^l	145.0 (9)	O2^xl—Cs1—O2^lx	84.9 (6)
O1^xiii—Cs1—O2^li	90.1 (9)	O2^xl—Cs1—O2^lxi	121.1 (8)
O1^xiii—Cs1—O2^lii	109.0 (8)	O2^xl—Cs1—O2^lxii	58.9 (8)
O1^xiii—Cs1—O2^liv	60.3 (9)	O2^xl—Cs1—O2^lxiii	95.1 (6)
O1^xiii—Cs1—O2^lv	71.0 (8)	O2^xl—Cs1—O2^lxiv	19.3 (9)
O1^xiii—Cs1—O2^lvi	89.9 (9)	O2^xl—Cs1—O2^lxv	80.8 (9)
O1^xiii—Cs1—O2^lvii	90.2 (6)	O2^xl—Cs1—O2^lxvi	110.8 (7)
O1^xiii—Cs1—O2^lix	99.5 (7)	O2^xl—Cs1—O2^lxvii	110.8 (7)
O1^xiii—Cs1—O2^lxi	170.5 (9)	O2^xl—Cs1—O2^lxviii	150.5 (6)
O1^xiii—Cs1—O2^lxii	89.8 (6)	O2^xl—Cs1—O2^lxix	69.2 (7)
O1^xiii—Cs1—O2^lxiii	145.6 (10)	O2^xl—Cs1—O2^lxx	99.2 (9)
O1^xiii—Cs1—O2^lxiv	80.5 (7)	O2^xl—Cs1—O2^lxxi	29.5 (6)
O1^xiii—Cs1—O2^lxv	112.5 (6)	O2^xl—Cs1—O2^lxxii	69.2 (7)
O1^xiii—Cs1—O2^lxvi	52.5 (10)	O2^xli—Cs1—O2^xlii	91.9 (7)
O1^xiii—Cs1—O2^lxvii	151.2 (9)	O2^xli—Cs1—O2^xliii	42.0 (7)
O1^xiii—Cs1—O2^lxviii	83.4 (7)	O2^xli—Cs1—O2^xliv	106.9 (9)
O1^xiii—Cs1—O2^lxix	127.5 (10)	O2^xli—Cs1—O2^xlv	88.1 (7)
O1^xiii—Cs1—O2^lxx	67.5 (6)	O2^xli—Cs1—O2^xlvi	180
O1^xiii—Cs1—O2^lxxi	96.6 (7)	O2^xli—Cs1—O2^xlvii	73.1 (9)
O1^xiii—Cs1—O2^lxxii	28.8 (9)	O2^xli—Cs1—O2^xlviii	138.0 (7)
O1^xiv—Cs1—O1^xv	87.1 (3)	O2^xli—Cs1—O2^xlix	58.9 (8)
O1^xiv—Cs1—O1^xvi	87.1 (3)	O2^xli—Cs1—O2^l	121.1 (8)
O1^xiv—Cs1—O1^xvii	154.0 (11)	O2^xli—Cs1—O2^li	19.3 (9)
O1^xiv—Cs1—O1^xviii	61.7 (9)	O2^xli—Cs1—O2^lii	95.1 (6)
O1^xiv—Cs1—O1^xix	118.3 (9)	O2^xli—Cs1—O2^liii	58.9 (8)
O1^xiv—Cs1—O1^xx	38.3 (10)	O2^xli—Cs1—O2^liv	121.1 (8)
O1^xiv—Cs1—O1^xxi	99.5 (9)	O2^xli—Cs1—O2^lv	84.9 (6)
O1^xiv—Cs1—O1^xxii	80.5 (9)	O2^xli—Cs1—O2^lvi	160.7 (9)
O1^xiv—Cs1—O1^xxiii	141.7 (10)	O2^xli—Cs1—O2^lvii	29.5 (6)
O1^xiv—Cs1—O1^xxiv	61.7 (9)	O2^xli—Cs1—O2^lviii	69.2 (7)
O1^xiv—Cs1—O1^xxv	118.3 (9)	O2^xli—Cs1—O2^lix	69.2 (7)
O1^xiv—Cs1—O2^xxvi	89.8 (6)	O2^xli—Cs1—O2^lx	99.2 (9)
O1^xiv—Cs1—O2^xxvii	170.5 (9)	O2^xli—Cs1—O2^lxi	110.8 (7)
O1^xiv—Cs1—O2^xxviii	80.5 (7)	O2^xli—Cs1—O2^lxii	150.5 (6)
O1^xiv—Cs1—O2ⁱ	145.6 (10)	O2^xli—Cs1—O2^lxiii	80.8 (9)
O1^xiv—Cs1—O2^xxx	90.2 (6)	O2^xli—Cs1—O2^lxiv	110.8 (7)
O1^xiv—Cs1—O2^xxxii	99.5 (7)	O2^xli—Cs1—O2^lxv	170.0 (9)
O1^xiv—Cs1—O2^xxxiii	28.8 (9)	O2^xli—Cs1—O2^lxvi	97.4 (9)
O1^xiv—Cs1—O2^xxxiv	96.6 (7)	O2^xli—Cs1—O2^lxvii	136.7 (8)
O1^xiv—Cs1—O2^xxxv	67.5 (6)	O2^xli—Cs1—O2^lxviii	82.6 (9)
O1^xiv—Cs1—O2^xxxvi	127.5 (10)	O2^xli—Cs1—O2^lxix	82.6 (9)
O1^xiv—Cs1—O2^xxxvii	83.4 (7)	O2^xli—Cs1—O2^lxx	10.0 (9)
O1^xiv—Cs1—O2^xxxviii	151.2 (9)	O2^xli—Cs1—O2^lxxi	97.4 (9)
O1^xiv—Cs1—O2^xxxix	52.5 (10)	O2^xli—Cs1—O2^lxxii	43.3 (8)
O1^xiv—Cs1—O2^xl	112.5 (6)	O2^xlii—Cs1—O2^xliii	106.9 (9)
O1^xiv—Cs1—O2^xli	109.0 (8)	O2^xlii—Cs1—O2^xliv	42.0 (7)
O1^xiv—Cs1—O2^xlii	90.1 (9)	O2^xlii—Cs1—O2^xlv	180
O1^xiv—Cs1—O2^xliii	145.0 (9)	O2^xlii—Cs1—O2^xlvi	88.1 (7)
O1^xiv—Cs1—O2^xliv	119.7 (9)	O2^xlii—Cs1—O2^xlvii	138.0 (7)
O1^xiv—Cs1—O2^xlv	89.9 (9)	O2^xlii—Cs1—O2^xlviii	73.1 (9)
O1^xiv—Cs1—O2^xlvi	71.0 (8)	O2^xlii—Cs1—O2^xlix	121.1 (8)
O1^xiv—Cs1—O2^xlvii	60.3 (9)	O2^xlii—Cs1—O2^l	58.9 (8)
O1^xiv—Cs1—O2^xlix	60.3 (9)	O2^xlii—Cs1—O2^li	95.1 (6)
O1^xiv—Cs1—O2^li	89.9 (9)	O2^xlii—Cs1—O2^lii	19.3 (9)
O1^xiv—Cs1—O2^lii	71.0 (8)	O2^xlii—Cs1—O2^liii	121.1 (8)
O1^xiv—Cs1—O2^liii	145.0 (9)	O2^xlii—Cs1—O2^liv	58.9 (8)
O1^xiv—Cs1—O2^liv	119.7 (9)	O2^xlii—Cs1—O2^lv	160.7 (9)
O1^xiv—Cs1—O2^lv	109.0 (8)	O2^xlii—Cs1—O2^lvi	84.9 (6)
O1^xiv—Cs1—O2^lvi	90.1 (9)	O2^xlii—Cs1—O2^lvii	69.2 (7)
O1^xiv—Cs1—O2^lvii	89.8 (6)	O2^xlii—Cs1—O2^lviii	99.2 (9)
O1^xiv—Cs1—O2^lviii	170.5 (9)	O2^xlii—Cs1—O2^lix	29.5 (6)
O1^xiv—Cs1—O2^lix	80.5 (7)	O2^xlii—Cs1—O2^lx	69.2 (7)
O1^xiv—Cs1—O2^lx	145.6 (10)	O2^xlii—Cs1—O2^lxi	80.8 (9)
O1^xiv—Cs1—O2^lxii	90.2 (6)	O2^xlii—Cs1—O2^lxii	110.8 (7)
O1^xiv—Cs1—O2^lxiv	99.5 (7)	O2^xlii—Cs1—O2^lxiii	110.8 (7)
O1^xiv—Cs1—O2^lxvi	127.5 (10)	O2^xlii—Cs1—O2^lxiv	150.5 (6)
O1^xiv—Cs1—O2^lxviii	96.6 (7)	O2^xlii—Cs1—O2^lxv	97.4 (9)
O1^xiv—Cs1—O2^lxix	52.5 (10)	O2^xlii—Cs1—O2^lxvi	43.3 (8)
O1^xiv—Cs1—O2^lxx	112.5 (6)	O2^xlii—Cs1—O2^lxvii	82.6 (9)
O1^xiv—Cs1—O2^lxxii	151.2 (9)	O2^xlii—Cs1—O2^lxviii	10.0 (9)
O1^xv—Cs1—O1^xvi	154.0 (11)	O2^xlii—Cs1—O2^lxix	136.7 (8)
O1^xv—Cs1—O1^xvii	87.1 (3)	O2^xlii—Cs1—O2^lxx	82.6 (9)
O1^xv—Cs1—O1^xviii	118.3 (9)	O2^xlii—Cs1—O2^lxxi	170.0 (9)
O1^xv—Cs1—O1^xix	61.7 (9)	O2^xlii—Cs1—O2^lxxii	97.4 (9)
O1^xv—Cs1—O1^xx	99.5 (9)	O2^xliii—Cs1—O2^xliv	91.9 (7)
O1^xv—Cs1—O1^xxi	38.3 (10)	O2^xliii—Cs1—O2^xlv	73.1 (9)
O1^xv—Cs1—O1^xxii	141.7 (10)	O2^xliii—Cs1—O2^xlvi	138.0 (7)
O1^xv—Cs1—O1^xxiii	80.5 (9)	O2^xliii—Cs1—O2^xlvii	88.1 (7)
O1^xv—Cs1—O1^xxiv	118.3 (9)	O2^xliii—Cs1—O2^xlviii	180
O1^xv—Cs1—O1^xxv	61.7 (9)	O2^xliii—Cs1—O2^xlix	84.9 (6)
O1^xv—Cs1—O2^xxvi	34.4 (10)	O2^xliii—Cs1—O2^l	160.7 (9)
O1^xv—Cs1—O2^xxvii	99.5 (7)	O2^xliii—Cs1—O2^li	58.9 (8)
O1^xv—Cs1—O2ⁱ	90.2 (6)	O2^xliii—Cs1—O2^lii	121.1 (8)
O1^xv—Cs1—O2^xxx	145.6 (10)	O2^xliii—Cs1—O2^liii	19.3 (9)
O1^xv—Cs1—O2^xxxi	89.8 (6)	O2^xliii—Cs1—O2^liv	95.1 (6)
O1^xv—Cs1—O2^xxxii	170.5 (9)	O2^xliii—Cs1—O2^lv	58.9 (8)
O1^xv—Cs1—O2^xxxiii	96.6 (7)	O2^xliii—Cs1—O2^lvi	121.1 (8)
O1^xv—Cs1—O2^xxxv	127.5 (10)	O2^xliii—Cs1—O2^lvii	69.2 (7)
O1^xv—Cs1—O2^xxxvi	67.5 (6)	O2^xliii—Cs1—O2^lviii	29.5 (6)
O1^xv—Cs1—O2^xxxvii	151.2 (9)	O2^xliii—Cs1—O2^lix	99.2 (9)
O1^xv—Cs1—O2^xxxviii	83.4 (7)	O2^xliii—Cs1—O2^lx	69.2 (7)
O1^xv—Cs1—O2^xxxix	112.5 (6)	O2^xliii—Cs1—O2^lxi	150.5 (6)
O1^xv—Cs1—O2^xl	52.5 (10)	O2^xliii—Cs1—O2^lxii	110.8 (7)
O1^xv—Cs1—O2^xli	145.0 (9)	O2^xliii—Cs1—O2^lxiii	110.8 (7)
O1^xv—Cs1—O2^xlii	119.7 (9)	O2^xliii—Cs1—O2^lxiv	80.8 (9)
O1^xv—Cs1—O2^xliii	109.0 (8)	O2^xliii—Cs1—O2^lxv	136.7 (8)
O1^xv—Cs1—O2^xliv	90.1 (9)	O2^xliii—Cs1—O2^lxvi	82.6 (9)
O1^xv—Cs1—O2^xlv	60.3 (9)	O2^xliii—Cs1—O2^lxvii	170.0 (9)
O1^xv—Cs1—O2^xlvi	35.0 (9)	O2^xliii—Cs1—O2^lxviii	97.4 (9)
O1^xv—Cs1—O2^xlvii	89.9 (9)	O2^xliii—Cs1—O2^lxix	97.4 (9)
O1^xv—Cs1—O2^xlviii	71.0 (8)	O2^xliii—Cs1—O2^lxx	43.3 (8)
O1^xv—Cs1—O2^xlix	109.0 (8)	O2^xliii—Cs1—O2^lxxi	82.6 (9)
O1^xv—Cs1—O2^l	90.1 (9)	O2^xliii—Cs1—O2^lxxii	10.0 (9)
O1^xv—Cs1—O2^li	145.0 (9)	O2^xliv—Cs1—O2^xlv	138.0 (7)
O1^xv—Cs1—O2^lii	119.7 (9)	O2^xliv—Cs1—O2^xlvi	73.1 (9)
O1^xv—Cs1—O2^liii	89.9 (9)	O2^xliv—Cs1—O2^xlvii	180
O1^xv—Cs1—O2^liv	71.0 (8)	O2^xliv—Cs1—O2^xlviii	88.1 (7)
O1^xv—Cs1—O2^lv	60.3 (9)	O2^xliv—Cs1—O2^xlix	160.7 (9)
O1^xv—Cs1—O2^lvii	170.5 (9)	O2^xliv—Cs1—O2^l	84.9 (6)
O1^xv—Cs1—O2^lviii	89.8 (6)	O2^xliv—Cs1—O2^li	121.1 (8)
O1^xv—Cs1—O2^lix	145.6 (10)	O2^xliv—Cs1—O2^lii	58.9 (8)
O1^xv—Cs1—O2^lx	80.5 (7)	O2^xliv—Cs1—O2^liii	95.1 (6)
O1^xv—Cs1—O2^lxi	90.2 (6)	O2^xliv—Cs1—O2^liv	19.3 (9)
O1^xv—Cs1—O2^lxii	9.5 (9)	O2^xliv—Cs1—O2^lv	121.1 (8)
O1^xv—Cs1—O2^lxiii	99.5 (7)	O2^xliv—Cs1—O2^lvi	58.9 (8)
O1^xv—Cs1—O2^lxiv	34.4 (10)	O2^xliv—Cs1—O2^lvii	99.2 (9)
O1^xv—Cs1—O2^lxv	28.8 (9)	O2^xliv—Cs1—O2^lviii	69.2 (7)
O1^xv—Cs1—O2^lxvi	96.6 (7)	O2^xliv—Cs1—O2^lix	69.2 (7)
O1^xv—Cs1—O2^lxvii	67.5 (6)	O2^xliv—Cs1—O2^lx	29.5 (6)
O1^xv—Cs1—O2^lxviii	127.5 (10)	O2^xliv—Cs1—O2^lxi	110.8 (7)
O1^xv—Cs1—O2^lxix	83.4 (7)	O2^xliv—Cs1—O2^lxii	80.8 (9)
O1^xv—Cs1—O2^lxx	151.2 (9)	O2^xliv—Cs1—O2^lxiii	150.5 (6)
O1^xv—Cs1—O2^lxxi	52.5 (10)	O2^xliv—Cs1—O2^lxiv	110.8 (7)
O1^xv—Cs1—O2^lxxii	112.5 (6)	O2^xliv—Cs1—O2^lxv	82.6 (9)
O1^xvi—Cs1—O1^xvii	87.1 (3)	O2^xliv—Cs1—O2^lxvi	10.0 (9)
O1^xvi—Cs1—O1^xviii	80.5 (9)	O2^xliv—Cs1—O2^lxvii	97.4 (9)
O1^xvi—Cs1—O1^xix	141.7 (10)	O2^xliv—Cs1—O2^lxviii	43.3 (8)
O1^xvi—Cs1—O1^xx	61.7 (9)	O2^xliv—Cs1—O2^lxix	170.0 (9)
O1^xvi—Cs1—O1^xxi	118.3 (9)	O2^xliv—Cs1—O2^lxx	97.4 (9)
O1^xvi—Cs1—O1^xxii	61.7 (9)	O2^xliv—Cs1—O2^lxxi	136.7 (8)
O1^xvi—Cs1—O1^xxiii	118.3 (9)	O2^xliv—Cs1—O2^lxxii	82.6 (9)
O1^xvi—Cs1—O1^xxv	99.5 (9)	O2^xlv—Cs1—O2^xlvi	91.9 (7)
O1^xvi—Cs1—O2^xxvi	170.5 (9)	O2^xlv—Cs1—O2^xlvii	42.0 (7)
O1^xvi—Cs1—O2^xxvii	89.8 (6)	O2^xlv—Cs1—O2^xlviii	106.9 (9)
O1^xvi—Cs1—O2^xxviii	145.6 (10)	O2^xlv—Cs1—O2^xlix	58.9 (8)
O1^xvi—Cs1—O2ⁱ	80.5 (7)	O2^xlv—Cs1—O2^l	121.1 (8)
O1^xvi—Cs1—O2^xxix	90.2 (6)	O2^xlv—Cs1—O2^li	84.9 (6)
O1^xvi—Cs1—O2^xxxi	99.5 (7)	O2^xlv—Cs1—O2^lii	160.7 (9)
O1^xvi—Cs1—O2^xxxii	34.4 (10)	O2^xlv—Cs1—O2^liii	58.9 (8)
O1^xvi—Cs1—O2^xxxiii	67.5 (6)	O2^xlv—Cs1—O2^liv	121.1 (8)
O1^xvi—Cs1—O2^xxxiv	127.5 (10)	O2^xlv—Cs1—O2^lv	19.3 (9)
O1^xvi—Cs1—O2^xxxv	28.8 (9)	O2^xlv—Cs1—O2^lvi	95.1 (6)
O1^xvi—Cs1—O2^xxxvi	96.6 (7)	O2^xlv—Cs1—O2^lvii	110.8 (7)
O1^xvi—Cs1—O2^xxxvii	52.5 (10)	O2^xlv—Cs1—O2^lviii	80.8 (9)
O1^xvi—Cs1—O2^xxxviii	112.5 (6)	O2^xlv—Cs1—O2^lix	150.5 (6)
O1^xvi—Cs1—O2^xxxix	83.4 (7)	O2^xlv—Cs1—O2^lx	110.8 (7)
O1^xvi—Cs1—O2^xl	151.2 (9)	O2^xlv—Cs1—O2^lxi	99.2 (9)
O1^xvi—Cs1—O2^xli	60.3 (9)	O2^xlv—Cs1—O2^lxii	69.2 (7)
O1^xvi—Cs1—O2^xlii	35.0 (9)	O2^xlv—Cs1—O2^lxiii	69.2 (7)
O1^xvi—Cs1—O2^xliii	89.9 (9)	O2^xlv—Cs1—O2^lxiv	29.5 (6)
O1^xvi—Cs1—O2^xliv	71.0 (8)	O2^xlv—Cs1—O2^lxv	82.6 (9)
O1^xvi—Cs1—O2^xlv	145.0 (9)	O2^xlv—Cs1—O2^lxvi	136.7 (8)
O1^xvi—Cs1—O2^xlvi	119.7 (9)	O2^xlv—Cs1—O2^lxvii	97.4 (9)
O1^xvi—Cs1—O2^xlvii	109.0 (8)	O2^xlv—Cs1—O2^lxviii	170.0 (9)
O1^xvi—Cs1—O2^xlviii	90.1 (9)	O2^xlv—Cs1—O2^lxix	43.3 (8)
O1^xvi—Cs1—O2^xlix	89.9 (9)	O2^xlv—Cs1—O2^lxx	97.4 (9)
O1^xvi—Cs1—O2^l	71.0 (8)	O2^xlv—Cs1—O2^lxxi	10.0 (9)
O1^xvi—Cs1—O2^li	60.3 (9)	O2^xlv—Cs1—O2^lxxii	82.6 (9)
O1^xvi—Cs1—O2^lii	35.0 (9)	O2^xlvi—Cs1—O2^xlvii	106.9 (9)
O1^xvi—Cs1—O2^liii	109.0 (8)	O2^xlvi—Cs1—O2^xlviii	42.0 (7)
O1^xvi—Cs1—O2^liv	90.1 (9)	O2^xlvi—Cs1—O2^xlix	121.1 (8)
O1^xvi—Cs1—O2^lv	145.0 (9)	O2^xlvi—Cs1—O2^l	58.9 (8)
O1^xvi—Cs1—O2^lvi	119.7 (9)	O2^xlvi—Cs1—O2^li	160.7 (9)
O1^xvi—Cs1—O2^lvii	34.4 (10)	O2^xlvi—Cs1—O2^lii	84.9 (6)
O1^xvi—Cs1—O2^lviii	99.5 (7)	O2^xlvi—Cs1—O2^liii	121.1 (8)
O1^xvi—Cs1—O2^lx	90.2 (6)	O2^xlvi—Cs1—O2^liv	58.9 (8)
O1^xvi—Cs1—O2^lxi	80.5 (7)	O2^xlvi—Cs1—O2^lv	95.1 (6)
O1^xvi—Cs1—O2^lxii	145.6 (10)	O2^xlvi—Cs1—O2^lvi	19.3 (9)
O1^xvi—Cs1—O2^lxiii	89.8 (6)	O2^xlvi—Cs1—O2^lvii	150.5 (6)
O1^xvi—Cs1—O2^lxiv	170.5 (9)	O2^xlvi—Cs1—O2^lviii	110.8 (7)
O1^xvi—Cs1—O2^lxv	127.5 (10)	O2^xlvi—Cs1—O2^lix	110.8 (7)
O1^xvi—Cs1—O2^lxvi	67.5 (6)	O2^xlvi—Cs1—O2^lx	80.8 (9)
O1^xvi—Cs1—O2^lxvii	96.6 (7)	O2^xlvi—Cs1—O2^lxi	69.2 (7)
O1^xvi—Cs1—O2^lxviii	28.8 (9)	O2^xlvi—Cs1—O2^lxii	29.5 (6)
O1^xvi—Cs1—O2^lxix	112.5 (6)	O2^xlvi—Cs1—O2^lxiii	99.2 (9)
O1^xvi—Cs1—O2^lxx	52.5 (10)	O2^xlvi—Cs1—O2^lxiv	69.2 (7)
O1^xvi—Cs1—O2^lxxi	151.2 (9)	O2^xlvi—Cs1—O2^lxv	10.0 (9)
O1^xvi—Cs1—O2^lxxii	83.4 (7)	O2^xlvi—Cs1—O2^lxvi	82.6 (9)
O1^xvii—Cs1—O1^xviii	141.7 (10)	O2^xlvi—Cs1—O2^lxvii	43.3 (8)
O1^xvii—Cs1—O1^xix	80.5 (9)	O2^xlvi—Cs1—O2^lxviii	97.4 (9)
O1^xvii—Cs1—O1^xx	118.3 (9)	O2^xlvi—Cs1—O2^lxix	97.4 (9)
O1^xvii—Cs1—O1^xxi	61.7 (9)	O2^xlvi—Cs1—O2^lxx	170.0 (9)
O1^xvii—Cs1—O1^xxii	118.3 (9)	O2^xlvi—Cs1—O2^lxxi	82.6 (9)
O1^xvii—Cs1—O1^xxiii	61.7 (9)	O2^xlvi—Cs1—O2^lxxii	136.7 (8)
O1^xvii—Cs1—O1^xxiv	99.5 (9)	O2^xlvii—Cs1—O2^xlviii	91.9 (7)
O1^xvii—Cs1—O1^xxv	38.3 (10)	O2^xlvii—Cs1—O2^xlix	19.3 (9)
O1^xvii—Cs1—O2^xxvi	99.5 (7)	O2^xlvii—Cs1—O2^l	95.1 (6)
O1^xvii—Cs1—O2^xxviii	90.2 (6)	O2^xlvii—Cs1—O2^li	58.9 (8)
O1^xvii—Cs1—O2^xxix	145.6 (10)	O2^xlvii—Cs1—O2^lii	121.1 (8)
O1^xvii—Cs1—O2^xxx	80.5 (7)	O2^xlvii—Cs1—O2^liii	84.9 (6)
O1^xvii—Cs1—O2^xxxi	170.5 (9)	O2^xlvii—Cs1—O2^liv	160.7 (9)
O1^xvii—Cs1—O2^xxxii	89.8 (6)	O2^xlvii—Cs1—O2^lv	58.9 (8)
O1^xvii—Cs1—O2^xxxiii	127.5 (10)	O2^xlvii—Cs1—O2^lvi	121.1 (8)
O1^xvii—Cs1—O2^xxxiv	67.5 (6)	O2^xlvii—Cs1—O2^lvii	80.8 (9)
O1^xvii—Cs1—O2^xxxv	96.6 (7)	O2^xlvii—Cs1—O2^lviii	110.8 (7)
O1^xvii—Cs1—O2^xxxvi	28.8 (9)	O2^xlvii—Cs1—O2^lix	110.8 (7)
O1^xvii—Cs1—O2^xxxvii	112.5 (6)	O2^xlvii—Cs1—O2^lx	150.5 (6)
O1^xvii—Cs1—O2^xxxviii	52.5 (10)	O2^xlvii—Cs1—O2^lxi	69.2 (7)
O1^xvii—Cs1—O2^xxxix	151.2 (9)	O2^xlvii—Cs1—O2^lxii	99.2 (9)
O1^xvii—Cs1—O2^xl	83.4 (7)	O2^xlvii—Cs1—O2^lxiii	29.5 (6)
O1^xvii—Cs1—O2^xli	89.9 (9)	O2^xlvii—Cs1—O2^lxiv	69.2 (7)
O1^xvii—Cs1—O2^xlii	71.0 (8)	O2^xlvii—Cs1—O2^lxv	97.4 (9)
O1^xvii—Cs1—O2^xliii	60.3 (9)	O2^xlvii—Cs1—O2^lxvi	170.0 (9)
O1^xvii—Cs1—O2^xlv	109.0 (8)	O2^xlvii—Cs1—O2^lxvii	82.6 (9)
O1^xvii—Cs1—O2^xlvi	90.1 (9)	O2^xlvii—Cs1—O2^lxviii	136.7 (8)
O1^xvii—Cs1—O2^xlvii	145.0 (9)	O2^xlvii—Cs1—O2^lxix	10.0 (9)
O1^xvii—Cs1—O2^xlviii	119.7 (9)	O2^xlvii—Cs1—O2^lxx	82.6 (9)
O1^xvii—Cs1—O2^xlix	145.0 (9)	O2^xlvii—Cs1—O2^lxxi	43.3 (8)
O1^xvii—Cs1—O2^l	119.7 (9)	O2^xlvii—Cs1—O2^lxxii	97.4 (9)
O1^xvii—Cs1—O2^li	109.0 (8)	O2^xlviii—Cs1—O2^xlix	95.1 (6)
O1^xvii—Cs1—O2^lii	90.1 (9)	O2^xlviii—Cs1—O2^l	19.3 (9)
O1^xvii—Cs1—O2^liii	60.3 (9)	O2^xlviii—Cs1—O2^li	121.1 (8)
O1^xvii—Cs1—O2^lv	89.9 (9)	O2^xlviii—Cs1—O2^lii	58.9 (8)
O1^xvii—Cs1—O2^lvi	71.0 (8)	O2^xlviii—Cs1—O2^liii	160.7 (9)
O1^xvii—Cs1—O2^lvii	99.5 (7)	O2^xlviii—Cs1—O2^liv	84.9 (6)
O1^xvii—Cs1—O2^lix	90.2 (6)	O2^xlviii—Cs1—O2^lv	121.1 (8)
O1^xvii—Cs1—O2^lxi	145.6 (10)	O2^xlviii—Cs1—O2^lvi	58.9 (8)
O1^xvii—Cs1—O2^lxii	80.5 (7)	O2^xlviii—Cs1—O2^lvii	110.8 (7)
O1^xvii—Cs1—O2^lxiii	170.5 (9)	O2^xlviii—Cs1—O2^lviii	150.5 (6)
O1^xvii—Cs1—O2^lxiv	89.8 (6)	O2^xlviii—Cs1—O2^lix	80.8 (9)
O1^xvii—Cs1—O2^lxv	96.6 (7)	O2^xlviii—Cs1—O2^lx	110.8 (7)
O1^xvii—Cs1—O2^lxvi	28.8 (9)	O2^xlviii—Cs1—O2^lxi	29.5 (6)
O1^xvii—Cs1—O2^lxvii	127.5 (10)	O2^xlviii—Cs1—O2^lxii	69.2 (7)
O1^xvii—Cs1—O2^lxviii	67.5 (6)	O2^xlviii—Cs1—O2^lxiii	69.2 (7)
O1^xvii—Cs1—O2^lxix	151.2 (9)	O2^xlviii—Cs1—O2^lxiv	99.2 (9)
O1^xvii—Cs1—O2^lxx	83.4 (7)	O2^xlviii—Cs1—O2^lxv	43.3 (8)
O1^xvii—Cs1—O2^lxxi	112.5 (6)	O2^xlviii—Cs1—O2^lxvi	97.4 (9)
O1^xvii—Cs1—O2^lxxii	52.5 (10)	O2^xlviii—Cs1—O2^lxvii	10.0 (9)
O1^xviii—Cs1—O1^xix	87.1 (3)	O2^xlviii—Cs1—O2^lxviii	82.6 (9)
O1^xviii—Cs1—O1^xx	87.1 (3)	O2^xlviii—Cs1—O2^lxix	82.6 (9)
O1^xviii—Cs1—O1^xxi	154.0 (11)	O2^xlviii—Cs1—O2^lxx	136.7 (8)
O1^xviii—Cs1—O1^xxiii	92.9 (3)	O2^xlviii—Cs1—O2^lxxi	97.4 (9)
O1^xviii—Cs1—O1^xxiv	92.9 (3)	O2^xlviii—Cs1—O2^lxxii	170.0 (9)
O1^xviii—Cs1—O1^xxv	180	O2^xlix—Cs1—O2^l	91.9 (7)
O1^xviii—Cs1—O2^xxvi	90.1 (9)	O2^xlix—Cs1—O2^li	42.0 (7)
O1^xviii—Cs1—O2^xxvii	109.0 (8)	O2^xlix—Cs1—O2^lii	106.9 (9)
O1^xviii—Cs1—O2^xxviii	119.7 (9)	O2^xlix—Cs1—O2^liii	88.1 (7)
O1^xviii—Cs1—O2ⁱ	145.0 (9)	O2^xlix—Cs1—O2^liv	180
O1^xviii—Cs1—O2^xxix	71.0 (8)	O2^xlix—Cs1—O2^lv	73.1 (9)
O1^xviii—Cs1—O2^xxx	89.9 (9)	O2^xlix—Cs1—O2^lvi	138.0 (7)
O1^xviii—Cs1—O2^xxxii	60.3 (9)	O2^xlix—Cs1—O2^lvii	61.8 (9)
O1^xviii—Cs1—O2^xxxiii	80.5 (7)	O2^xlix—Cs1—O2^lviii	112.6 (7)
O1^xviii—Cs1—O2^xxxiv	145.6 (10)	O2^xlix—Cs1—O2^lix	92.5 (8)
O1^xviii—Cs1—O2^xxxv	89.8 (6)	O2^xlix—Cs1—O2^lx	154.1 (7)
O1^xviii—Cs1—O2^xxxvi	170.5 (9)	O2^xlix—Cs1—O2^lxi	67.4 (7)
O1^xviii—Cs1—O2^xxxvii	34.4 (10)	O2^xlix—Cs1—O2^lxii	118.2 (9)
O1^xviii—Cs1—O2^xxxviii	99.5 (7)	O2^xlix—Cs1—O2^lxiii	25.9 (7)
O1^xviii—Cs1—O2^xl	90.2 (6)	O2^xlix—Cs1—O2^lxiv	87.5 (8)
O1^xviii—Cs1—O2^xli	52.5 (10)	O2^xlix—Cs1—O2^lxv	112.6 (7)
O1^xviii—Cs1—O2^xlii	112.5 (6)	O2^xlix—Cs1—O2^lxvi	154.1 (7)
O1^xviii—Cs1—O2^xliii	83.4 (7)	O2^xlix—Cs1—O2^lxvii	87.5 (8)
O1^xviii—Cs1—O2^xliv	151.2 (9)	O2^xlix—Cs1—O2^lxviii	118.2 (9)
O1^xviii—Cs1—O2^xlv	67.5 (6)	O2^xlix—Cs1—O2^lxix	25.9 (7)
O1^xviii—Cs1—O2^xlvi	127.5 (10)	O2^xlix—Cs1—O2^lxx	67.4 (7)
O1^xviii—Cs1—O2^xlviii	96.6 (7)	O2^xlix—Cs1—O2^lxxi	61.8 (9)
O1^xviii—Cs1—O2^l	90.2 (6)	O2^xlix—Cs1—O2^lxxii	92.5 (8)
O1^xviii—Cs1—O2^lii	99.5 (7)	O2^l—Cs1—O2^li	106.9 (9)
O1^xviii—Cs1—O2^liii	89.8 (6)	O2^l—Cs1—O2^lii	42.0 (7)
O1^xviii—Cs1—O2^liv	170.5 (9)	O2^l—Cs1—O2^liii	180
O1^xviii—Cs1—O2^lv	80.5 (7)	O2^l—Cs1—O2^liv	88.1 (7)
O1^xviii—Cs1—O2^lvi	145.6 (10)	O2^l—Cs1—O2^lv	138.0 (7)
O1^xviii—Cs1—O2^lvii	52.5 (10)	O2^l—Cs1—O2^lvi	73.1 (9)
O1^xviii—Cs1—O2^lviii	112.5 (6)	O2^l—Cs1—O2^lvii	92.5 (8)
O1^xviii—Cs1—O2^lix	83.4 (7)	O2^l—Cs1—O2^lviii	154.1 (7)
O1^xviii—Cs1—O2^lx	151.2 (9)	O2^l—Cs1—O2^lix	61.8 (9)
O1^xviii—Cs1—O2^lxi	67.5 (6)	O2^l—Cs1—O2^lx	112.6 (7)
O1^xviii—Cs1—O2^lxii	127.5 (10)	O2^l—Cs1—O2^lxi	25.9 (7)
O1^xviii—Cs1—O2^lxiii	28.8 (9)	O2^l—Cs1—O2^lxii	87.5 (8)
O1^xviii—Cs1—O2^lxiv	96.6 (7)	O2^l—Cs1—O2^lxiii	67.4 (7)
O1^xviii—Cs1—O2^lxv	119.7 (9)	O2^l—Cs1—O2^lxiv	118.2 (9)
O1^xviii—Cs1—O2^lxvi	145.0 (9)	O2^l—Cs1—O2^lxv	61.8 (9)
O1^xviii—Cs1—O2^lxvii	90.1 (9)	O2^l—Cs1—O2^lxvi	92.5 (8)
O1^xviii—Cs1—O2^lxviii	109.0 (8)	O2^l—Cs1—O2^lxvii	25.9 (7)
O1^xviii—Cs1—O2^lxx	60.3 (9)	O2^l—Cs1—O2^lxviii	67.4 (7)
O1^xviii—Cs1—O2^lxxi	71.0 (8)	O2^l—Cs1—O2^lxix	87.5 (8)
O1^xviii—Cs1—O2^lxxii	89.9 (9)	O2^l—Cs1—O2^lxx	118.2 (9)
O1^xix—Cs1—O1^xx	154.0 (11)	O2^l—Cs1—O2^lxxi	112.6 (7)
O1^xix—Cs1—O1^xxi	87.1 (3)	O2^l—Cs1—O2^lxxii	154.1 (7)
O1^xix—Cs1—O1^xxii	92.9 (3)	O2^li—Cs1—O2^lii	91.9 (7)
O1^xix—Cs1—O1^xxiv	180	O2^li—Cs1—O2^liii	73.1 (9)
O1^xix—Cs1—O1^xxv	92.9 (3)	O2^li—Cs1—O2^liv	138.0 (7)
O1^xix—Cs1—O2^xxvii	60.3 (9)	O2^li—Cs1—O2^lv	88.1 (7)
O1^xix—Cs1—O2^xxviii	71.0 (8)	O2^li—Cs1—O2^lvi	180
O1^xix—Cs1—O2ⁱ	89.9 (9)	O2^li—Cs1—O2^lvii	25.9 (7)
O1^xix—Cs1—O2^xxix	119.7 (9)	O2^li—Cs1—O2^lviii	87.5 (8)
O1^xix—Cs1—O2^xxx	145.0 (9)	O2^li—Cs1—O2^lix	67.4 (7)
O1^xix—Cs1—O2^xxxi	90.1 (9)	O2^li—Cs1—O2^lx	118.2 (9)
O1^xix—Cs1—O2^xxxii	109.0 (8)	O2^li—Cs1—O2^lxi	92.5 (8)
O1^xix—Cs1—O2^xxxiii	145.6 (10)	O2^li—Cs1—O2^lxii	154.1 (7)
O1^xix—Cs1—O2^xxxiv	80.5 (7)	O2^li—Cs1—O2^lxiii	61.8 (9)
O1^xix—Cs1—O2^xxxv	170.5 (9)	O2^li—Cs1—O2^lxiv	112.6 (7)
O1^xix—Cs1—O2^xxxvi	89.8 (6)	O2^li—Cs1—O2^lxv	154.1 (7)
O1^xix—Cs1—O2^xxxvii	99.5 (7)	O2^li—Cs1—O2^lxvi	112.6 (7)
O1^xix—Cs1—O2^xxxix	90.2 (6)	O2^li—Cs1—O2^lxvii	118.2 (9)
O1^xix—Cs1—O2^xl	9.5 (9)	O2^li—Cs1—O2^lxviii	87.5 (8)
O1^xix—Cs1—O2^xli	83.4 (7)	O2^li—Cs1—O2^lxix	67.4 (7)
O1^xix—Cs1—O2^xlii	151.2 (9)	O2^li—Cs1—O2^lxx	25.9 (7)
O1^xix—Cs1—O2^xliii	52.5 (10)	O2^li—Cs1—O2^lxxi	92.5 (8)
O1^xix—Cs1—O2^xliv	112.5 (6)	O2^li—Cs1—O2^lxxii	61.8 (9)
O1^xix—Cs1—O2^xlvi	96.6 (7)	O2^lii—Cs1—O2^liii	138.0 (7)
O1^xix—Cs1—O2^xlvii	67.5 (6)	O2^lii—Cs1—O2^liv	73.1 (9)
O1^xix—Cs1—O2^xlviii	127.5 (10)	O2^lii—Cs1—O2^lv	180
O1^xix—Cs1—O2^xlix	80.5 (7)	O2^lii—Cs1—O2^lvi	88.1 (7)
O1^xix—Cs1—O2^l	145.6 (10)	O2^lii—Cs1—O2^lvii	67.4 (7)
O1^xix—Cs1—O2^li	89.8 (6)	O2^lii—Cs1—O2^lviii	118.2 (9)
O1^xix—Cs1—O2^lii	170.5 (9)	O2^lii—Cs1—O2^lix	25.9 (7)
O1^xix—Cs1—O2^liii	34.4 (10)	O2^lii—Cs1—O2^lx	87.5 (8)
O1^xix—Cs1—O2^liv	99.5 (7)	O2^lii—Cs1—O2^lxi	61.8 (9)
O1^xix—Cs1—O2^lv	9.5 (9)	O2^lii—Cs1—O2^lxii	112.6 (7)
O1^xix—Cs1—O2^lvi	90.2 (6)	O2^lii—Cs1—O2^lxiii	92.5 (8)
O1^xix—Cs1—O2^lvii	112.5 (6)	O2^lii—Cs1—O2^lxiv	154.1 (7)
O1^xix—Cs1—O2^lviii	52.5 (10)	O2^lii—Cs1—O2^lxv	92.5 (8)
O1^xix—Cs1—O2^lix	151.2 (9)	O2^lii—Cs1—O2^lxvi	61.8 (9)
O1^xix—Cs1—O2^lx	83.4 (7)	O2^lii—Cs1—O2^lxvii	67.4 (7)
O1^xix—Cs1—O2^lxi	127.5 (10)	O2^lii—Cs1—O2^lxviii	25.9 (7)
O1^xix—Cs1—O2^lxii	67.5 (6)	O2^lii—Cs1—O2^lxix	118.2 (9)
O1^xix—Cs1—O2^lxiii	96.6 (7)	O2^lii—Cs1—O2^lxx	87.5 (8)
O1^xix—Cs1—O2^lxv	90.1 (9)	O2^lii—Cs1—O2^lxxi	154.1 (7)
O1^xix—Cs1—O2^lxvi	109.0 (8)	O2^lii—Cs1—O2^lxxii	112.6 (7)
O1^xix—Cs1—O2^lxvii	119.7 (9)	O2^liii—Cs1—O2^liv	91.9 (7)
O1^xix—Cs1—O2^lxviii	145.0 (9)	O2^liii—Cs1—O2^lv	42.0 (7)
O1^xix—Cs1—O2^lxix	71.0 (8)	O2^liii—Cs1—O2^lvi	106.9 (9)
O1^xix—Cs1—O2^lxx	89.9 (9)	O2^liii—Cs1—O2^lvii	87.5 (8)
O1^xix—Cs1—O2^lxxi	35.0 (9)	O2^liii—Cs1—O2^lviii	25.9 (7)
O1^xix—Cs1—O2^lxxii	60.3 (9)	O2^liii—Cs1—O2^lix	118.2 (9)
O1^xx—Cs1—O1^xxi	87.1 (3)	O2^liii—Cs1—O2^lx	67.4 (7)
O1^xx—Cs1—O1^xxii	92.9 (3)	O2^liii—Cs1—O2^lxi	154.1 (7)
O1^xx—Cs1—O1^xxiii	180	O2^liii—Cs1—O2^lxii	92.5 (8)
O1^xx—Cs1—O1^xxv	92.9 (3)	O2^liii—Cs1—O2^lxiii	112.6 (7)
O1^xx—Cs1—O2^xxvi	119.7 (9)	O2^liii—Cs1—O2^lxiv	61.8 (9)
O1^xx—Cs1—O2^xxvii	145.0 (9)	O2^liii—Cs1—O2^lxv	118.2 (9)
O1^xx—Cs1—O2^xxviii	90.1 (9)	O2^liii—Cs1—O2^lxvi	87.5 (8)
O1^xx—Cs1—O2ⁱ	109.0 (8)	O2^liii—Cs1—O2^lxvii	154.1 (7)
O1^xx—Cs1—O2^xxx	60.3 (9)	O2^liii—Cs1—O2^lxviii	112.6 (7)
O1^xx—Cs1—O2^xxxi	71.0 (8)	O2^liii—Cs1—O2^lxix	92.5 (8)
O1^xx—Cs1—O2^xxxii	89.9 (9)	O2^liii—Cs1—O2^lxx	61.8 (9)
O1^xx—Cs1—O2^xxxiv	90.2 (6)	O2^liii—Cs1—O2^lxxi	67.4 (7)
O1^xx—Cs1—O2^xxxvi	99.5 (7)	O2^liii—Cs1—O2^lxxii	25.9 (7)
O1^xx—Cs1—O2^xxxvii	89.8 (6)	O2^liv—Cs1—O2^lv	106.9 (9)
O1^xx—Cs1—O2^xxxviii	170.5 (9)	O2^liv—Cs1—O2^lvi	42.0 (7)
O1^xx—Cs1—O2^xxxix	80.5 (7)	O2^liv—Cs1—O2^lvii	118.2 (9)
O1^xx—Cs1—O2^xl	145.6 (10)	O2^liv—Cs1—O2^lviii	67.4 (7)
O1^xx—Cs1—O2^xli	112.5 (6)	O2^liv—Cs1—O2^lix	87.5 (8)
O1^xx—Cs1—O2^xlii	52.5 (10)	O2^liv—Cs1—O2^lx	25.9 (7)
O1^xx—Cs1—O2^xliii	151.2 (9)	O2^liv—Cs1—O2^lxi	112.6 (7)
O1^xx—Cs1—O2^xliv	83.4 (7)	O2^liv—Cs1—O2^lxii	61.8 (9)
O1^xx—Cs1—O2^xlv	127.5 (10)	O2^liv—Cs1—O2^lxiii	154.1 (7)
O1^xx—Cs1—O2^xlvi	67.5 (6)	O2^liv—Cs1—O2^lxiv	92.5 (8)
O1^xx—Cs1—O2^xlvii	96.6 (7)	O2^liv—Cs1—O2^lxv	67.4 (7)
O1^xx—Cs1—O2^xlviii	28.8 (9)	O2^liv—Cs1—O2^lxvi	25.9 (7)
O1^xx—Cs1—O2^xlix	90.2 (6)	O2^liv—Cs1—O2^lxvii	92.5 (8)
O1^xx—Cs1—O2^l	9.5 (9)	O2^liv—Cs1—O2^lxviii	61.8 (9)
O1^xx—Cs1—O2^li	99.5 (7)	O2^liv—Cs1—O2^lxix	154.1 (7)
O1^xx—Cs1—O2^liii	170.5 (9)	O2^liv—Cs1—O2^lxx	112.6 (7)
O1^xx—Cs1—O2^liv	89.8 (6)	O2^liv—Cs1—O2^lxxi	118.2 (9)
O1^xx—Cs1—O2^lv	145.6 (10)	O2^liv—Cs1—O2^lxxii	87.5 (8)
O1^xx—Cs1—O2^lvi	80.5 (7)	O2^lv—Cs1—O2^lvi	91.9 (7)
O1^xx—Cs1—O2^lvii	83.4 (7)	O2^lv—Cs1—O2^lvii	112.6 (7)
O1^xx—Cs1—O2^lviii	151.2 (9)	O2^lv—Cs1—O2^lviii	61.8 (9)
O1^xx—Cs1—O2^lix	52.5 (10)	O2^lv—Cs1—O2^lix	154.1 (7)
O1^xx—Cs1—O2^lx	112.5 (6)	O2^lv—Cs1—O2^lx	92.5 (8)
O1^xx—Cs1—O2^lxi	28.8 (9)	O2^lv—Cs1—O2^lxi	118.2 (9)
O1^xx—Cs1—O2^lxii	96.6 (7)	O2^lv—Cs1—O2^lxii	67.4 (7)
O1^xx—Cs1—O2^lxiii	67.5 (6)	O2^lv—Cs1—O2^lxiii	87.5 (8)
O1^xx—Cs1—O2^lxiv	127.5 (10)	O2^lv—Cs1—O2^lxiv	25.9 (7)
O1^xx—Cs1—O2^lxv	71.0 (8)	O2^lv—Cs1—O2^lxv	87.5 (8)
O1^xx—Cs1—O2^lxvi	89.9 (9)	O2^lv—Cs1—O2^lxvi	118.2 (9)
O1^xx—Cs1—O2^lxvii	35.0 (9)	O2^lv—Cs1—O2^lxvii	112.6 (7)
O1^xx—Cs1—O2^lxviii	60.3 (9)	O2^lv—Cs1—O2^lxviii	154.1 (7)
O1^xx—Cs1—O2^lxix	90.1 (9)	O2^lv—Cs1—O2^lxix	61.8 (9)
O1^xx—Cs1—O2^lxx	109.0 (8)	O2^lv—Cs1—O2^lxx	92.5 (8)
O1^xx—Cs1—O2^lxxi	119.7 (9)	O2^lv—Cs1—O2^lxxi	25.9 (7)
O1^xx—Cs1—O2^lxxii	145.0 (9)	O2^lv—Cs1—O2^lxxii	67.4 (7)
O1^xxi—Cs1—O1^xxii	180	O2^lvi—Cs1—O2^lvii	154.1 (7)
O1^xxi—Cs1—O1^xxiii	92.9 (3)	O2^lvi—Cs1—O2^lviii	92.5 (8)
O1^xxi—Cs1—O1^xxiv	92.9 (3)	O2^lvi—Cs1—O2^lix	112.6 (7)
O1^xxi—Cs1—O1^xxv	26.0 (11)	O2^lvi—Cs1—O2^lx	61.8 (9)
O1^xxi—Cs1—O2^xxvi	71.0 (8)	O2^lvi—Cs1—O2^lxi	87.5 (8)
O1^xxi—Cs1—O2^xxvii	89.9 (9)	O2^lvi—Cs1—O2^lxii	25.9 (7)
O1^xxi—Cs1—O2ⁱ	60.3 (9)	O2^lvi—Cs1—O2^lxiii	118.2 (9)
O1^xxi—Cs1—O2^xxix	90.1 (9)	O2^lvi—Cs1—O2^lxiv	67.4 (7)
O1^xxi—Cs1—O2^xxx	109.0 (8)	O2^lvi—Cs1—O2^lxv	25.9 (7)
O1^xxi—Cs1—O2^xxxi	119.7 (9)	O2^lvi—Cs1—O2^lxvi	67.4 (7)
O1^xxi—Cs1—O2^xxxii	145.0 (9)	O2^lvi—Cs1—O2^lxvii	61.8 (9)
O1^xxi—Cs1—O2^xxxiii	90.2 (6)	O2^lvi—Cs1—O2^lxviii	92.5 (8)
O1^xxi—Cs1—O2^xxxiv	9.5 (9)	O2^lvi—Cs1—O2^lxix	112.6 (7)
O1^xxi—Cs1—O2^xxxv	99.5 (7)	O2^lvi—Cs1—O2^lxx	154.1 (7)
O1^xxi—Cs1—O2^xxxvi	34.4 (10)	O2^lvi—Cs1—O2^lxxi	87.5 (8)
O1^xxi—Cs1—O2^xxxvii	170.5 (9)	O2^lvi—Cs1—O2^lxxii	118.2 (9)
O1^xxi—Cs1—O2^xxxviii	89.8 (6)	O2^lvii—Cs1—O2^lviii	91.9 (7)
O1^xxi—Cs1—O2^xxxix	145.6 (10)	O2^lvii—Cs1—O2^lix	42.0 (7)
O1^xxi—Cs1—O2^xl	80.5 (7)	O2^lvii—Cs1—O2^lx	106.9 (9)
O1^xxi—Cs1—O2^xli	151.2 (9)	O2^lvii—Cs1—O2^lxi	88.1 (7)
O1^xxi—Cs1—O2^xlii	83.4 (7)	O2^lvii—Cs1—O2^lxii	180
O1^xxi—Cs1—O2^xliii	112.5 (6)	O2^lvii—Cs1—O2^lxiii	73.1 (9)
O1^xxi—Cs1—O2^xliv	52.5 (10)	O2^lvii—Cs1—O2^lxiv	138.0 (7)
O1^xxi—Cs1—O2^xlv	96.6 (7)	O2^lvii—Cs1—O2^lxv	154.1 (7)
O1^xxi—Cs1—O2^xlvi	28.8 (9)	O2^lvii—Cs1—O2^lxvi	92.5 (8)
O1^xxi—Cs1—O2^xlvii	127.5 (10)	O2^lvii—Cs1—O2^lxvii	112.6 (7)
O1^xxi—Cs1—O2^xlviii	67.5 (6)	O2^lvii—Cs1—O2^lxviii	61.8 (9)
O1^xxi—Cs1—O2^xlix	145.6 (10)	O2^lvii—Cs1—O2^lxix	87.5 (8)
O1^xxi—Cs1—O2^l	80.5 (7)	O2^lvii—Cs1—O2^lxx	25.9 (7)
O1^xxi—Cs1—O2^li	170.5 (9)	O2^lvii—Cs1—O2^lxxi	118.2 (9)
O1^xxi—Cs1—O2^lii	89.8 (6)	O2^lvii—Cs1—O2^lxxii	67.4 (7)
O1^xxi—Cs1—O2^liii	99.5 (7)	O2^lviii—Cs1—O2^lix	106.9 (9)
O1^xxi—Cs1—O2^lv	90.2 (6)	O2^lviii—Cs1—O2^lx	42.0 (7)
O1^xxi—Cs1—O2^lvii	151.2 (9)	O2^lviii—Cs1—O2^lxi	180
O1^xxi—Cs1—O2^lviii	83.4 (7)	O2^lviii—Cs1—O2^lxii	88.1 (7)
O1^xxi—Cs1—O2^lix	112.5 (6)	O2^lviii—Cs1—O2^lxiii	138.0 (7)
O1^xxi—Cs1—O2^lx	52.5 (10)	O2^lviii—Cs1—O2^lxiv	73.1 (9)
O1^xxi—Cs1—O2^lxi	96.6 (7)	O2^lviii—Cs1—O2^lxv	112.6 (7)
O1^xxi—Cs1—O2^lxiii	127.5 (10)	O2^lviii—Cs1—O2^lxvi	61.8 (9)
O1^xxi—Cs1—O2^lxiv	67.5 (6)	O2^lviii—Cs1—O2^lxvii	154.1 (7)
O1^xxi—Cs1—O2^lxvii	71.0 (8)	O2^lviii—Cs1—O2^lxviii	92.5 (8)
O1^xxi—Cs1—O2^lxviii	89.9 (9)	O2^lviii—Cs1—O2^lxix	118.2 (9)
O1^xxi—Cs1—O2^lxix	119.7 (9)	O2^lviii—Cs1—O2^lxx	67.4 (7)
O1^xxi—Cs1—O2^lxx	145.0 (9)	O2^lviii—Cs1—O2^lxxi	87.5 (8)
O1^xxi—Cs1—O2^lxxi	90.1 (9)	O2^lviii—Cs1—O2^lxxii	25.9 (7)
O1^xxi—Cs1—O2^lxxii	109.0 (8)	O2^lix—Cs1—O2^lx	91.9 (7)
O1^xxii—Cs1—O1^xxiii	87.1 (3)	O2^lix—Cs1—O2^lxi	73.1 (9)
O1^xxii—Cs1—O1^xxiv	87.1 (3)	O2^lix—Cs1—O2^lxii	138.0 (7)
O1^xxii—Cs1—O1^xxv	154.0 (11)	O2^lix—Cs1—O2^lxiii	88.1 (7)
O1^xxii—Cs1—O2^xxvi	109.0 (8)	O2^lix—Cs1—O2^lxiv	180
O1^xxii—Cs1—O2^xxvii	90.1 (9)	O2^lix—Cs1—O2^lxv	118.2 (9)
O1^xxii—Cs1—O2^xxviii	145.0 (9)	O2^lix—Cs1—O2^lxvi	67.4 (7)
O1^xxii—Cs1—O2ⁱ	119.7 (9)	O2^lix—Cs1—O2^lxvii	87.5 (8)
O1^xxii—Cs1—O2^xxix	89.9 (9)	O2^lix—Cs1—O2^lxviii	25.9 (7)
O1^xxii—Cs1—O2^xxx	71.0 (8)	O2^lix—Cs1—O2^lxix	112.6 (7)
O1^xxii—Cs1—O2^xxxi	60.3 (9)	O2^lix—Cs1—O2^lxx	61.8 (9)
O1^xxii—Cs1—O2^xxxii	35.0 (9)	O2^lix—Cs1—O2^lxxi	154.1 (7)
O1^xxii—Cs1—O2^xxxiii	89.8 (6)	O2^lix—Cs1—O2^lxxii	92.5 (8)
O1^xxii—Cs1—O2^xxxiv	170.5 (9)	O2^lx—Cs1—O2^lxi	138.0 (7)
O1^xxii—Cs1—O2^xxxv	80.5 (7)	O2^lx—Cs1—O2^lxii	73.1 (9)
O1^xxii—Cs1—O2^xxxvi	145.6 (10)	O2^lx—Cs1—O2^lxiii	180
O1^xxii—Cs1—O2^xxxviii	90.2 (6)	O2^lx—Cs1—O2^lxiv	88.1 (7)
O1^xxii—Cs1—O2^xl	99.5 (7)	O2^lx—Cs1—O2^lxv	87.5 (8)
O1^xxii—Cs1—O2^xlii	96.6 (7)	O2^lx—Cs1—O2^lxvi	25.9 (7)
O1^xxii—Cs1—O2^xliii	67.5 (6)	O2^lx—Cs1—O2^lxvii	118.2 (9)
O1^xxii—Cs1—O2^xliv	127.5 (10)	O2^lx—Cs1—O2^lxviii	67.4 (7)
O1^xxii—Cs1—O2^xlv	83.4 (7)	O2^lx—Cs1—O2^lxix	154.1 (7)
O1^xxii—Cs1—O2^xlvi	151.2 (9)	O2^lx—Cs1—O2^lxx	92.5 (8)
O1^xxii—Cs1—O2^xlvii	52.5 (10)	O2^lx—Cs1—O2^lxxi	112.6 (7)
O1^xxii—Cs1—O2^xlviii	112.5 (6)	O2^lx—Cs1—O2^lxxii	61.8 (9)
O1^xxii—Cs1—O2^l	99.5 (7)	O2^lxi—Cs1—O2^lxii	91.9 (7)
O1^xxii—Cs1—O2^lii	90.2 (6)	O2^lxi—Cs1—O2^lxiii	42.0 (7)
O1^xxii—Cs1—O2^liii	80.5 (7)	O2^lxi—Cs1—O2^lxiv	106.9 (9)
O1^xxii—Cs1—O2^liv	145.6 (10)	O2^lxi—Cs1—O2^lxv	67.4 (7)
O1^xxii—Cs1—O2^lv	89.8 (6)	O2^lxi—Cs1—O2^lxvi	118.2 (9)
O1^xxii—Cs1—O2^lvi	170.5 (9)	O2^lxi—Cs1—O2^lxvii	25.9 (7)
O1^xxii—Cs1—O2^lvii	28.8 (9)	O2^lxi—Cs1—O2^lxviii	87.5 (8)
O1^xxii—Cs1—O2^lviii	96.6 (7)	O2^lxi—Cs1—O2^lxix	61.8 (9)
O1^xxii—Cs1—O2^lix	67.5 (6)	O2^lxi—Cs1—O2^lxx	112.6 (7)
O1^xxii—Cs1—O2^lx	127.5 (10)	O2^lxi—Cs1—O2^lxxi	92.5 (8)
O1^xxii—Cs1—O2^lxi	83.4 (7)	O2^lxi—Cs1—O2^lxxii	154.1 (7)
O1^xxii—Cs1—O2^lxii	151.2 (9)	O2^lxii—Cs1—O2^lxiii	106.9 (9)
O1^xxii—Cs1—O2^lxiii	52.5 (10)	O2^lxii—Cs1—O2^lxiv	42.0 (7)
O1^xxii—Cs1—O2^lxiv	112.5 (6)	O2^lxii—Cs1—O2^lxv	25.9 (7)
O1^xxii—Cs1—O2^lxv	145.0 (9)	O2^lxii—Cs1—O2^lxvi	87.5 (8)
O1^xxii—Cs1—O2^lxvi	119.7 (9)	O2^lxii—Cs1—O2^lxvii	67.4 (7)
O1^xxii—Cs1—O2^lxvii	109.0 (8)	O2^lxii—Cs1—O2^lxviii	118.2 (9)
O1^xxii—Cs1—O2^lxviii	90.1 (9)	O2^lxii—Cs1—O2^lxix	92.5 (8)
O1^xxii—Cs1—O2^lxix	60.3 (9)	O2^lxii—Cs1—O2^lxx	154.1 (7)
O1^xxii—Cs1—O2^lxxi	89.9 (9)	O2^lxii—Cs1—O2^lxxi	61.8 (9)
O1^xxii—Cs1—O2^lxxii	71.0 (8)	O2^lxii—Cs1—O2^lxxii	112.6 (7)
O1^xxiii—Cs1—O1^xxiv	154.0 (11)	O2^lxiii—Cs1—O2^lxiv	91.9 (7)
O1^xxiii—Cs1—O1^xxv	87.1 (3)	O2^lxiii—Cs1—O2^lxv	92.5 (8)
O1^xxiii—Cs1—O2^xxvi	60.3 (9)	O2^lxiii—Cs1—O2^lxvi	154.1 (7)
O1^xxiii—Cs1—O2^xxvii	35.0 (9)	O2^lxiii—Cs1—O2^lxvii	61.8 (9)
O1^xxiii—Cs1—O2^xxviii	89.9 (9)	O2^lxiii—Cs1—O2^lxviii	112.6 (7)
O1^xxiii—Cs1—O2ⁱ	71.0 (8)	O2^lxiii—Cs1—O2^lxix	25.9 (7)
O1^xxiii—Cs1—O2^xxix	145.0 (9)	O2^lxiii—Cs1—O2^lxx	87.5 (8)
O1^xxiii—Cs1—O2^xxx	119.7 (9)	O2^lxiii—Cs1—O2^lxxi	67.4 (7)
O1^xxiii—Cs1—O2^xxxi	109.0 (8)	O2^lxiii—Cs1—O2^lxxii	118.2 (9)
O1^xxiii—Cs1—O2^xxxii	90.1 (9)	O2^lxiv—Cs1—O2^lxv	61.8 (9)
O1^xxiii—Cs1—O2^xxxiii	170.5 (9)	O2^lxiv—Cs1—O2^lxvi	112.6 (7)
O1^xxiii—Cs1—O2^xxxiv	89.8 (6)	O2^lxiv—Cs1—O2^lxvii	92.5 (8)
O1^xxiii—Cs1—O2^xxxv	145.6 (10)	O2^lxiv—Cs1—O2^lxviii	154.1 (7)
O1^xxiii—Cs1—O2^xxxvi	80.5 (7)	O2^lxiv—Cs1—O2^lxix	67.4 (7)
O1^xxiii—Cs1—O2^xxxvii	90.2 (6)	O2^lxiv—Cs1—O2^lxx	118.2 (9)
O1^xxiii—Cs1—O2^xxxix	99.5 (7)	O2^lxiv—Cs1—O2^lxxi	25.9 (7)
O1^xxiii—Cs1—O2^xl	34.4 (10)	O2^lxiv—Cs1—O2^lxxii	87.5 (8)
O1^xxiii—Cs1—O2^xli	67.5 (6)	O2^lxv—Cs1—O2^lxvi	91.9 (7)
O1^xxiii—Cs1—O2^xlii	127.5 (10)	O2^lxv—Cs1—O2^lxvii	42.0 (7)
O1^xxiii—Cs1—O2^xliii	28.8 (9)	O2^lxv—Cs1—O2^lxviii	106.9 (9)
O1^xxiii—Cs1—O2^xliv	96.6 (7)	O2^lxv—Cs1—O2^lxix	88.1 (7)
O1^xxiii—Cs1—O2^xlv	52.5 (10)	O2^lxv—Cs1—O2^lxx	180
O1^xxiii—Cs1—O2^xlvi	112.5 (6)	O2^lxv—Cs1—O2^lxxi	73.1 (9)
O1^xxiii—Cs1—O2^xlvii	83.4 (7)	O2^lxv—Cs1—O2^lxxii	138.0 (7)
O1^xxiii—Cs1—O2^xlviii	151.2 (9)	O2^lxvi—Cs1—O2^lxvii	106.9 (9)
O1^xxiii—Cs1—O2^xlix	89.8 (6)	O2^lxvi—Cs1—O2^lxviii	42.0 (7)
O1^xxiii—Cs1—O2^l	170.5 (9)	O2^lxvi—Cs1—O2^lxix	180
O1^xxiii—Cs1—O2^li	80.5 (7)	O2^lxvi—Cs1—O2^lxx	88.1 (7)
O1^xxiii—Cs1—O2^lii	145.6 (10)	O2^lxvi—Cs1—O2^lxxi	138.0 (7)
O1^xxiii—Cs1—O2^liv	90.2 (6)	O2^lxvi—Cs1—O2^lxxii	73.1 (9)
O1^xxiii—Cs1—O2^lv	34.4 (10)	O2^lxvii—Cs1—O2^lxviii	91.9 (7)
O1^xxiii—Cs1—O2^lvi	99.5 (7)	O2^lxvii—Cs1—O2^lxix	73.1 (9)
O1^xxiii—Cs1—O2^lvii	96.6 (7)	O2^lxvii—Cs1—O2^lxx	138.0 (7)
O1^xxiii—Cs1—O2^lviii	28.8 (9)	O2^lxvii—Cs1—O2^lxxi	88.1 (7)
O1^xxiii—Cs1—O2^lix	127.5 (10)	O2^lxvii—Cs1—O2^lxxii	180
O1^xxiii—Cs1—O2^lx	67.5 (6)	O2^lxviii—Cs1—O2^lxix	138.0 (7)
O1^xxiii—Cs1—O2^lxi	151.2 (9)	O2^lxviii—Cs1—O2^lxx	73.1 (9)
O1^xxiii—Cs1—O2^lxii	83.4 (7)	O2^lxviii—Cs1—O2^lxxi	180
O1^xxiii—Cs1—O2^lxiii	112.5 (6)	O2^lxviii—Cs1—O2^lxxii	88.1 (7)
O1^xxiii—Cs1—O2^lxiv	52.5 (10)	O2^lxix—Cs1—O2^lxx	91.9 (7)
O1^xxiii—Cs1—O2^lxv	109.0 (8)	O2^lxix—Cs1—O2^lxxii	106.9 (9)
O1^xxiii—Cs1—O2^lxvi	90.1 (9)	O2^lxx—Cs1—O2^lxxi	106.9 (9)
O1^xxiii—Cs1—O2^lxvii	145.0 (9)	O2^lxxi—Cs1—O2^lxxii	91.9 (7)
O1^xxiii—Cs1—O2^lxviii	119.7 (9)

Symmetry codes: (i) −x+1, −y+1, z; (ii) x−1, y−1, z−1; (iii) x−1, y, z−1; (iv) x, y−1, z−1; (v) x, y, z−1; (vi) −x, y−1, −z+1; (vii) −x, y, −z+1; (viii) −x+1, y−1, −z+1; (ix) −x+1, y, −z+1; (x) z−1, x−1, y−1; (xi) z−1, x−1, y; (xii) z−1, x, y−1; (xiii) z−1, x, y; (xiv) −z+1, −x, y−1; (xv) −z+1, −x, y; (xvi) −z+1, −x+1, y−1; (xvii) −z+1, −x+1, y; (xviii) y−1, z−1, x−1; (xix) y−1, z−1, x; (xx) y, z−1, x−1; (xxi) y, z−1, x; (xxii) y−1, −z+1, −x; (xxiii) y−1, −z+1, −x+1; (xxiv) y, −z+1, −x; (xxv) y, −z+1, −x+1; (xxvi) x−1, y−1, z; (xxvii) x−1, y, z; (xxviii) −x+1, −y, z; (xxix) −x+1, y−1, −z; (xxx) −x+1, y, −z; (xxxi) x−1, −y, −z; (xxxii) x−1, −y+1, −z; (xxxiii) z, x−1, y−1; (xxxiv) z, x−1, y; (xxxv) z, −x+1, −y; (xxxvi) z, −x+1, −y+1; (xxxvii) −z, −x+1, y−1; (xxxviii) −z, −x+1, y; (xxxix) −z, x−1, −y; (xl) −z, x−1, −y+1; (xli) y−1, z, x−1; (xlii) y, z, x−1; (xliii) −y, z, −x+1; (xliv) −y+1, z, −x+1; (xlv) y−1, −z, −x+1; (xlvi) y, −z, −x+1; (xlvii) −y, −z, x−1; (xlviii) −y+1, −z, x−1; (xlix) y−1, x−1, −z; (l) y, x−1, −z; (li) −y, −x+1, −z; (lii) −y+1, −x+1, −z; (liii) y−1, −x+1, z; (liv) y, −x+1, z; (lv) −y, x−1, z; (lvi) −y+1, x−1, z; (lvii) x−1, z, −y; (lviii) x−1, z, −y+1; (lix) −x+1, z, y−1; (lx) −x+1, z, y; (lxi) −x+1, −z, −y; (lxii) −x+1, −z, −y+1; (lxiii) x−1, −z, y−1; (lxiv) x−1, −z, y; (lxv) z, y−1, −x+1; (lxvi) z, y, −x+1; (lxvii) z, −y, x−1; (lxviii) z, −y+1, x−1; (lxix) −z, y−1, x−1; (lxx) −z, y, x−1; (lxxi) −z, −y, −x+1; (lxxii) −z, −y+1, −x+1.

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