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Determination of Composition and Anomeric Ratio in Mixtures of Fluorinated Ologosaccharides.

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    0521796 - ÚCHP 2020 CZ eng C - Konferenční příspěvek (zahraniční konf.)
    Červenková Šťastná, Lucie - Kurfiřt, Martin - Hamala, Vojtěch - Karban, Jindřich
    Determination of Composition and Anomeric Ratio in Mixtures of Fluorinated Ologosaccharides.
    Book of Abstracts. Prague: Institute of Chemical Process Fundamentals of the CAS, v. v. i., 2019, s. 63, č. článku P17. ISBN 978-80-86186-97-9.
    [Magnetic Moments in Central Europe 2019. Prague (CZ), 27.02.2019-03.03.2019]
    Grant CEP: GA MŠk(CZ) LM2015037
    Institucionální podpora: RVO:67985858
    Klíčová slova: deoxofluorinated oligosaccharides * glycosylation * 2D NMR techniques
    Kód oboru RIV: CC - Organická chemie
    Obor OECD: Organic chemistry

    Plenthora of glycosylation reactions was performed and sophisticated NMR approach for characteriza-tion of the coressponding products was aplied. ID 19F and *H NMR were utilized for accurate derermina-tion of anomeric ratios and 2D NMR techniques as HSQC, HMBC and COSY were used to assign the signals of individual anomers. In some cases, spectrum simulation was necessary to obtain the desired parameters.
    Trvalý link: http://hdl.handle.net/11104/0306362
    Název souboruStaženoVelikostKomentářVerzePřístup
    00206B6C274C200206081036.doc8270.8 KBVydavatelský postprintpovolen
     
Počet záznamů: 1