Počet záznamů: 1
Synthesis and characterization of new coordination polymer with l-proline amino acid ligand, new precursor for preparation of pure phase lead(II) oxide nanoparticles via thermal decomposition
- 1.0482858 - FZÚ 2018 RIV IR eng J - Článek v odborném periodiku
Varzdar, S. - Hashemi, L. - Morsali, A. - Dušek, Michal
Synthesis and characterization of new coordination polymer with l-proline amino acid ligand, new precursor for preparation of pure phase lead(II) oxide nanoparticles via thermal decomposition.
Journal of the Iranian Chemical Society. Roč. 14, č. 11 (2017), s. 2255-2261. ISSN 1735-207X. E-ISSN 1735-2428
Institucionální podpora: RVO:68378271
Klíčová slova: coordination polymer * nanoparticle * lead(II) oxide * proline amino acid
Obor OECD: Condensed matter physics (including formerly solid state physics, supercond.)
Impakt faktor: 1.593, rok: 2017
A new two-dimensional lead(II) coordination polymer, [Pb(Pro)2]n (1), Pro = l-proline amino acid, has been synthesized and characterized by IR and X-ray diffraction. Structural determination reveals the Pb(II) ion is four-coordinated, bonded to two nitrogen atoms and two oxygen atoms from the l-proline ligand. PbO nanoparticles were synthesized by calcination at 500, 550 and 600 °C under air atmosphere. The PbO nanostructure was characterized by scanning electron microscopy (SEM) and X-ray powder diffraction (XRD). The thermal stability was studied by thermal gravimetric analysis (TGA) and diffe rential thermal analysis (DTA).
Trvalý link: http://hdl.handle.net/11104/0278252
Počet záznamů: 1