Počet záznamů: 1  

Characterization and crystal structure of a 17-membered macrocyclic Schiff base compound MeO-sal-pn-bn

  1. 1. 0456422 - FZU-D 2016 RIV RU eng J - Článek v odborném periodiku
    Khalaji, A.D. - Ghoran, S.H. - Rohlíček, Jan - Dušek, Michal
    Characterization and crystal structure of a 17-membered macrocyclic Schiff base compound MeO-sal-pn-bn.
    Journal of Structural Chemistry. Roč. 56, č. 2 (2015), s. 259-265. ISSN 0022-4766
    Grant ostatní:AV ČR(CZ) AP0701
    Program:Akademická prémie - Praemium Academiae
    Institucionální podpora: RVO:68378271
    Klíčová slova: macrocyclic * Schiff base * spectroscopy * powder diffraction * orthorhombic
    Kód oboru RIV: BM - Fyzika pevných látek a magnetismus
    Impakt faktor: 0.536, rok: 2015

    The reaction of 1,4-diaminobutane with 2,2′-diformyl-6,6′-dimethoxy-diphenoxypropane in a mixed solvent of methanol and chloroform results in a new 17-membered macrocyclic Schiff base compound MeO-sal-pn-pn. The title compound is characterized by the elemental analysis (CHN), FT-IR, 1H NMR spectroscopy, and powder X-ray diffraction. The crystal data are: Mr = 396.5, orthorhombic, P212121, with unit cell parameters: a = 4.71769(3) Å, b = 19.1524(2) Å, c = 22.9418(2) Å, V = 2072.90(3) Å3, and Z = 4.
    Trvalý link: http://hdl.handle.net/11104/0256951