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Direct continuous supercritical fluid extraction as a novel method of wine analysis. Comparison with conventional indirect extraction and implications for wine variety identification
- 1.0162454 - UIACH-O 20033017 RIV NL eng J - Článek v odborném periodiku
Karásek, Pavel - Planeta, Josef - Varaďová-Ostrá, Elena - Mikešová, Milena - Goliáš, J. - Roth, Michal - Vejrosta, Jiří
Direct continuous supercritical fluid extraction as a novel method of wine analysis. Comparison with conventional indirect extraction and implications for wine variety identification.
Journal of Chromatography A. Roč. 1002, 1-2 (2003), s. 13-23. ISSN 0021-9673. E-ISSN 1873-3778
Grant CEP: GA ČR GA525/99/1570; GA AV ČR IBS4031110
Výzkumný záměr: CEZ:AV0Z4031919
Klíčová slova: supercritical fluid extraction * wine analysis * multivariate statistics
Kód oboru RIV: CB - Analytická chemie, separace
Impakt faktor: 2.922, rok: 2003
Direct supercritical fluid extraction (SFE) of wines with carbon dioxide was compared to SFE of the sorbent used for solid-phase extraction of the same wine samples (SPE-SFE). Compared to SPE-SFE, the direct SFE results in a more specific and representative gas chromatographic fingerprint of the wine sample. The multivariate statistical processing of the direct SFE-GC data provides a clear-cut and sharp discrimination among the individual wine varieties while the discrimination based on the SPE-SFE-GC data is relatively poor. This finding reflects the adverse effects of additional analytesorbent interactions and sorption/desorption steps involved in SPE-SFE.
Trvalý link: http://hdl.handle.net/11104/0059769
Počet záznamů: 1