Description of raw data for the article: Manuscript ID: DT-ART-11-2024-003267.R1 Title: High Temperature Interactions of Lead Palmitate with Linseed Oil Authors: Ruslan Barannikov (1,2), Joen Hermans (3,4,5), Jiøí Plocek (1), Petr Bezdièka (1), Anna Vykydalová (1), Andrii Mahun (6), Libor Kobera (6), Silvie Švarcová (1)* Affiliations: (1) Institute of Inorganic Chemistry of the Czech Academy of Sciences, Husinec 1001, 250 68 Husinec-üe§, Czech Republic (IIC CAS) (2) Department of Inorganic Chemistry, Faculty of Science, Charles University in Prague, Hlavova 2030/8, 128 40 Prague, Czech Republic (CU) (3) Van 't Hoff Institute for Molecular Sciences, University of Amsterdam, PO Box 94157, 1090GD Amsterdam, The Netherlands (UvA) (4) Conservation & Restoration, Amsterdam School of Heritage, Memory and Material Culture, University of Amsterdam, PO Box 94552, 1090GN Amsterdam, The Netherlands (UvA) (5) Conservation & Science, Rijksmuseum, Hobbemastraat 22, 1071ZC Amsterdam, The Netherlands (Rijksmuseum) (6) Institute of Macromolecular Chemistry of the Czech Academy of Sciences, Heyrovskeho nam. 2, 162 00, Prague 6, Czech Republic (IMC CAS) * corresponding author Journal: Dalton Transactions (submitted 22nd November 2024, accepted 4th Mach 2025) DOI: 10.1039/d4dt03267e Data description: Dataset contains diffraction patterns in xrdml format. The files can be open using the HighScore programme. Regarding ssNMR datasets, there are several software options for reading/analysing NMR data, both freeware and commercial: i.e. TopSpin and MestReNova. The "1r" file is a readable file with processed experimental data and the "title" file contains basic experimental information. Fig./Table No. Data type Sample code in the paper Raw data file Acquired at (Institution) Fig. 1 a,b DSC (1st heating) Pb(C16)2+LO_mix Pb(C16)2_LO_1.heat.txt IIC CAS Fig. 1 a,b DSC (2nd heating) Pb(C16)2+LO_mix Pb(C16)2_LO_2.heat.txt IIC CAS Fig. 1 a,b DSC (1st cooling) Pb(C16)2+LO_mix Pb(C16)2_LO_cooling.txt IIC CAS Fig. 2 a,b HT-XRPD (heating-start) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_25°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling-end) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_25°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_30°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_30°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_40°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_40°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_50°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_50°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_60°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_60°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_70°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_70°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_80°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_80°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_90°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_90°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_100°C_1.xrdml IIC CAS Fig. 2 a,b HT-XRPD (cooling) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_100°C_2.xrdml IIC CAS Fig. 2 a,b HT-XRPD (heating) Pb(C16)2+LO_mix PbC16-LO-2023-11-13_110°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_25°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_25°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_30°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_30°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_40°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_40°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_50°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_50°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_60°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_60°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_70°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_70°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_80°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_80°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_90°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_90°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_100°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_100°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_110°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_110°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_120°C_1.xrdml IIC CAS Fig. 2 c,d HT-XRPD (cooling) Pb(C16)2 Pb-Palmitate_HTXRD_120°C_2.xrdml IIC CAS Fig. 2 c,d HT-XRPD (heating) Pb(C16)2 Pb-Palmitate_HTXRD_130°C_2.xrdml IIC CAS Fig. 3 a,b HT-XRPD (25°C-start) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_25°C_1.xrdml IIC CAS Fig. 3 a,b HT-XRPD (25°C-end) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_25°C_2.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_0 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_1.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_10 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_2.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_20 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_3.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_30 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_4.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_40 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_5.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_50 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_6.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_60 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_7.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_70 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_8.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_80 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_9.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_90 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_10.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_100 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_11.xrdml IIC CAS Fig. 3 a,b HT-XRPD (112°C_110 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_12.xrdml IIC CAS Fig. 3 c,d HT-XRPD (25°C-start) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_25°C_1.xrdml IIC CAS Fig. 3 c,d HT-XRPD (25°C-end) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_25°C_2.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_0 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_1.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_10 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_2.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_20 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_3.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_30 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_4.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_40 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_5.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_50 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_6.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_60 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_7.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_70 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_8.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_80 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_9.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_90 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_10.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_100 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_11.xrdml IIC CAS Fig. 3 c,d HT-XRPD (112°C_110 min) Pb(C16)2 PbC16_pure_2024-02-28_HTXRD_112°C_12.xrdml IIC CAS Fig. 4 a HT-XRPD (112°C_110 min) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_112°C_12.xrdml IIC CAS Fig. 4 b HT-XRPD (25°C-end) Pb(C16)2+LO_mix PbC16_LO_2024-02-28_HTXRD_25°C_2.xrdml IIC CAS Fig. 5 a XRPD Pb(C16)2+LO_mix Pb-C16-LO-predTA-na-Si-Co.xrdml IIC CAS Fig. 5 a XRPD Pb(C16)2+LO_112°C PbC16-LO_1-3_afterTA-na-Si-Co.xrdml IIC CAS Fig. 5 b ATR-FTIR Pb(C16)2+LO_mix Pb(C16)2+LO_po TA_200723_ATR_diamant.CSV IIC CAS Fig. 5 b ATR-FTIR Pb(C16)2+LO_112°C Pb(C16)2+LO_pred TA_200723_ATR_diamant.CSV IIC CAS Fig. 7 ATR-FTIR Pb(C8)2 Pb(C8)2_RB_v01_ATR-diamant.CSV IIC CAS Fig. 7 ATR-FTIR Pb(C16)2+LO_112°C Pb(C16)2+LO_po TA_200723_ATR_diamant.CSV IIC CAS Fig. 7 HT-ATR-FTIR(25°C-150°C-25°C) Pb(C16)2 Pb-Palmitate 25-150-25.csv UvA Fig. 8, Table 3 ssNMR Pb(C16)2+LO_112°C ssNMR_PbC16LO.zip IMC CAS Fig. 8, Table 3 ssNMR Pb(C16)2+LO_112°C ssNMR_PbC16LO.zip IMC CAS Table 3 ssNMR Pb(C8)2 ssNMR_PbC8.zip IMC CAS Fig. 9, Fig. 10 XRPD (0 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_0.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (6 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_1.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (18 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_2.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (30 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_3.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (42 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_4.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (54 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_5.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (66 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_6.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (78 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_7.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (90 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_8.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (102 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_9.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (114 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_10.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (126 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_11.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (138 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_12.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (150 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_13.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (162 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_14.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (174 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_15.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (186 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_16.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (198 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_17.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (210 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_18.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (222 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_19.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (234 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_20.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (246 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_21.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (258 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_22.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (270 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_23.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (282 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_24.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (294 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_25.xrdml IIC CAS Fig. 9, Fig. 10 XRPD (306 hours) Pb(C16)2+LO_112°C Barannikov-PbC16-LO_1-3_110C-LN2-na-Si-Co-2024-01-30_26.xrdml IIC CAS Fig. 11 trans-FTIR (0 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_0_pokus1.CSV IIC CAS Fig. 11 trans-FTIR (24 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_1.CSV IIC CAS Fig. 11 trans-FTIR (48 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_2.CSV IIC CAS Fig. 11 trans-FTIR (72 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_3.CSV IIC CAS Fig. 11 trans-FTIR (96 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_4.CSV IIC CAS Fig. 11 trans-FTIR (120 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_5.CSV IIC CAS Fig. 11 trans-FTIR (144 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_6.CSV IIC CAS Fig. 11 trans-FTIR (168 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_7.CSV IIC CAS Fig. 11 trans-FTIR (192 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_8.CSV IIC CAS Fig. 11 trans-FTIR (216 hours) Pb(C16)2+LO_112°C PbC16_LO_po_300124_9.CSV IIC CAS